tribenzylaluminium*diethyl etherate

Base Information

Chemical Name:tribenzylaluminium*diethyl etherate
CAS No.:70827-66-6
Molecular Formula:C₂₅H₃₁AlO
Molecular Weight:374.502
Hs Code.:

Synonyms:

Suppliers and Price of tribenzylaluminium*diethyl etherate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tribenzylaluminium*diethyl etherate

Chemical Property:

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Technology Process of tribenzylaluminium*diethyl etherate

There total 2 articles about tribenzylaluminium*diethyl etherate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60-29-7,927820-24-4
diethyl ether

: 14994-03-7
tris(benzyl)aluminum

: 70827-66-6
tribenzylaluminium*diethyl etherate

Guidance literature:: In diethyl ether; benzene; (PhCH2)3Al was dissolved in a mixed benzene-ether solvent mixture; a portion of the solvent was slowly removed on the vac. system;
DOI:10.1016/0022-328X(87)83023-1

Reference yield:

: 780-24-5
dibenzylmercury(II)

: 70827-66-6
tribenzylaluminium*diethyl etherate

Guidance literature:: Multi-step reaction with 2 steps

1: xylene

2: benzene; diethyl ether

In diethyl ether; benzene;
DOI:10.1016/0022-328X(87)83023-1

Reference yield: 20.0%

: 70827-66-6
tribenzylaluminium*diethyl etherate

: 101009-34-1
trans-(Mo₆Cl₈)Cl₄(tributylphosphine)2

: 192516-66-8
tetrabenzyl-2κC,3κC,4κC,5κC-octa-μ3-chloro-bis(tributylphosphine)-1κP,6κP-octahedro-hexamolybdenum(12Mo-Mo)

Guidance literature:: In toluene; N2-atmosphere; addn. of excess of Al-compd. to Mo-complex soln., stirring (room temp., 1 d); filtration, solvent removal (vac.), crystn. (253 K), washing (ether);
DOI:10.1107/S0108270197002266