Combine the prepared 1,3-bis(silyloxy)-1,3-butadiene and 2-aryldiazenyl-3-silyloxy-2-en-1-one under suitable reaction conditions. The [3+3] cyclization involves the formation of three bonds between the diene and enone components, resulting in a cyclized product.
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3-(phenyldiazenyl)-4-(trimethylsilyloxy)pent-3-en-2-one
2-fluoro-1-(2-methoxyphenyl)-1,3-butanedione
