Literature Comparison

Continuously compare your results to published spectra and known chemical shifts for similar compounds. This can help verify your assignments.

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Chemical shifts Regioselectivity Green chemistry Characterization Coupling constants Yield NMR spectroscopy Distillation Decomposition Nucleophile reflux Deprotonation Chromatography Recrystallization Mass spectrometry (MS) Gas syringe Atom economy Electrophiles Protecting groups Deprotection GC (gas chromatography) Precursor Solvent polarity TLC (thin-layer chromatography) HPLC (high-performance liquid chromatography) Mechanistic Studies Product Isolation Workup Reaction Conditions Steric Effects Safety Precautions Reaction Mechanism Electronic effects Substrate Limitations Solvent Effects Substituent Effects Reaction Time Catalysis Catalyst Loading Reaction Monitoring Computational Chemistry Cryogenic Conditions Structure Confirmation Report the Results Literature Search Ethical Considerations Quenching Splitting Patterns NOE Experiments Extraction

Chemical Baike