103635-24-1

Basic information

• Product Name: 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-
• Synonyms: 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-
• CAS NO: 103635-24-1
• Molecular Formula: C17H16 N2 O2
• Molecular Weight: 0
• Mol File: 103635-24-1.mol

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-(CAS DataBase Reference)
• NIST Chemistry Reference: 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-(103635-24-1)
• EPA Substance Registry System: 4-Methoxybenzenamine, N-(2-benzylidenethylidenamino)-(103635-24-1)

Safety Data

• Hazardous Substances Data: 103635-24-1(Hazardous Substances Data)

Upstream product

• 3290-99-1 4-methoxybenzoic acid hydrazide 
• 104-55-2 3-phenyl-propenal 

Relevant articles and documents

METHOD FOR PREPAREING 1,3,4-OXADIAZOL UNDER SOLVENT-FREE CONDITION

The present invention relates to a synthesis method of 1,3,4-oxadiazol, comprising: 1) under a solvent-free condition and by means of a mechanical pulverization method, making a hydrazide compound react with an aldehyde compound and thereby synthesizing a N-acylhydrazone compound; and 2) under a solvent-free condition, adding an iodine-based oxidizing agent to the N-acylhydrazone compound to synthesize 1,3,4-oxadiazol via oxidative cyclization. The solventless synthesis method of 1,3,4-oxadiazol according to the present invention is easy to perform and handle, and has the advantage of synthesizing 1,3,4-oxadiazol at high selectivity and yield. Also, the solventless synthesis method of the present invention can prevent the formation of side products caused by the minute amount of water that usually remains in solvents, and can further prevent synthesized intermediates from being converted back into the starting materials by the water.COPYRIGHT KIPO 2016