104069-55-8Relevant articles and documents
Flow microwave technology and microreactors in synthesis
Baxendale, Ian R.,Hornung, Christian,Ley, Steven V.,De Mata Munoz Molina, Juan,Wikstroem, Anders
, p. 131 - 144 (2013/03/28)
A bespoke microwave reactor with a glass containment cell has been developed for performing continuous flow reactions under microwave heating. The prototype unit has been evaluated using a series of standard organic chemical transformations enabling scale-up of these chemical processes. As part of the development, a carbon-doped PTFE reactor insert was utilized to allow the heating of poorly absorbing reaction media, increasing the range of solvents and scope of reactions that can be performed in the device.
Synthesis of esters of lipophilic proline analogs by reduction of ethyl 5,6-dihydro-4H-1,2-oxazine-3-carboxylates
Henning,Lerch,Urbach
, p. 265 - 268 (2007/10/02)
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