1116005-16-3Relevant academic research and scientific papers
Gas chromatography analysis of reaction mixtures from cycloaddition reaction of α-ethylacroleine and ethyl ester α-ethylacrylic acid
Karpyak,Polyuzhyn,Marshalok,Yatchyshyn
, p. 397 - 401 (2008/09/20)
The gas chromatography (GC) method was applied for the analysis of reaction mixture from synthesis of 2-carboethoxy-2,5-diethyl-3,4-dihydro-2H-pyran. Relative errors of GC determinations not exceeded more than 7-8%. The reaction optimal conditions were proposed on the basis of such criteria as the conversion of α-ethylacrolein, yields and selectivities of main products by using the GC method.
