127923-96-0Relevant articles and documents
Reaction of 2-nitro-4-thiocyanatoaniline with 4-nitrochlorobenzene
Pilyugin,Chikisheva,Valitov,Sapozhnikov
, p. 1439 - 1443 (2002)
A method for preparing 4-amino-3,4′-dinitrodiphenyl sulfide is developed, based on the reaction of 2-nitro-4-thiocyanatoaniline with 4-nitrochlorobenzene in aqueous-alkaline medium in the presence of a phase-transfer catalyst (PEG 400 or Katamin AB).
Synthesis of 2-amino-5(6)-(4-aminophenyl)benzimidazole derivatives: II. Reaction of 2-nitro-4-thiocyanatoaniline with 4-nitrochlorobenzene
Pilyugin,Sapozhnikov,Shitov
, p. 979 - 984 (2007/10/03)
The reaction of 2-nitro-4-thiocyanatoaniline with 4-nitrochlorobenzene in aqueous alkaline medium in the presence of phase-transfer catalyst at 95-100°C was studied with a view to obtain 4-amino-3,4′- dinitrodiphenyl sulfide. Optimal conditions for the synthesis and isolation of the product were found.