1386972-65-1

Upstream product

• 1386972-62-8 2'-azidoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside 
• 28920-43-6 (fluorenylmethoxy)carbonyl chloride 
• 165331-08-8 (2R,3R,4S,5S,6R)-2-(2-Azido-ethoxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol 
• 604-69-3 β-D-glucose pentaacetate 

Downstream Products

• 1386972-56-0 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 4-O-[3-O-acetyl-4-O-benzyl-2-deoxy-6-O-(tert-butyldiphenylsilyl)-2-(trichloroethylcarbonylamino)-β-D-glucopyranosyl]-2,3,6-tri-O-benzyl-β-D-glucopyranoside 

Relevant academic research and scientific papers

Solid-phase synthesis of 2-aminoethyl glucosamine sulfoforms

Mono- and disaccharides of sulfonated glucosamines (GlcN sulfoforms) conjugated to 2-aminoethyl linkers were generated by solid-phase synthesis. Orthogonally protected intermediates were tethered onto tritylated polystyrene resin beads, subjected to amodular sequence of deprotection and sulfonation steps, then cleaved from solid support without degradation of N- or O-sulfate esters using solvolytic conditions, and finally purified by reverse-phase HPLC to afford the title compounds. Copyright Taylor & Francis Group, LLC.