2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1386972-65-1
Molecular Formula:C₄₄H₄₅NO₈
Molecular Weight:715.843
Hs Code.:

Synonyms:2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 5 articles about 2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₅NO₆

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1386972-65-1
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1080/07328303.2012.658274

Reference yield:

: 2-azidoethyl 4,6-O-benzylidene-β-D-glucopyranoside

: 1386972-65-1
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: triethylsilane; trifluorormethanesulfonic acid / dichloromethane / 6 h / -78 °C / Molecular sieve

3: tributylphosphine / dichloromethane; water / 27 h / 20 °C

4: sodium hydrogencarbonate / dichloromethane / 12 h / 0 - 20 °C

With triethylsilane; tributylphosphine; trifluorormethanesulfonic acid; sodium hydride; sodium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/07328303.2012.658274

Reference yield:

: 1386972-62-8
2'-azidoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

: 1386972-65-1
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tributylphosphine / dichloromethane; water / 27 h / 20 °C

2: sodium hydrogencarbonate / dichloromethane / 12 h / 0 - 20 °C

With tributylphosphine; sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1080/07328303.2012.658274