14928-77-9Relevant articles and documents
Efficient DBU accelerated synthesis of 18F-labelled trifluoroacetamides
Gómez, Antonio Bermejo,Cortés González, Miguel A.,Lübcke, Marvin,Johansson, Magnus J.,Halldin, Christer,Szabó, Kálmán J.,Schou, Magnus
supporting information, p. 13963 - 13966 (2016/12/09)
Nucleophilic 18F-fluorination of bromodifluoromethyl derivatives was performed using [18F]Bu4NF in the presence of DBU (1,8-diazabicyclo[5.4.0]undec-7-ene). This novel procedure provided a diverse set of [18F]trifluoroacetamides in good to excellent radiochemical conversions. A mechanism where DBU acts as organomediator in this transformation is proposed.
One-Step Hydroamidation of a Schiff Base with Trichlorosilane
Okamoto, Hidenori,Kato, Shozo
, p. 2128 - 2130 (2007/10/02)
We have found that the treatment of a Schiff base (2) with trichlorosilane and chloroacetyl chloride results in a highly active chloroacetamide herbicide (1) in an excellent yield .This one-step hydroamidation reaction of a Schiff base is a useful synthet