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15513-52-7

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15513-52-7 Usage

Chemical Properties

Off-white to tan powder

Uses

3-Nitro-2,6-lutidine may be used in the preparation of 3-methoxy-2,7-dimethyl-2H-1,4-diazepine1 and 3-amino-2,6-lutidine.

General Description

3-Nitro-2,6-lutidine, a nitropyridine derivative, is also known as 2,6-dimethyl-3-nitropyridine. It can be prepared from 2,6-lutidine via nitration.

Check Digit Verification of cas no

The CAS Registry Mumber 15513-52-7 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,5,5,1 and 3 respectively; the second part has 2 digits, 5 and 2 respectively.
Calculate Digit Verification of CAS Registry Number 15513-52:
(7*1)+(6*5)+(5*5)+(4*1)+(3*3)+(2*5)+(1*2)=87
87 % 10 = 7
So 15513-52-7 is a valid CAS Registry Number.
InChI:InChI=1/C7H8N2O2/c1-5-3-7(9(10)11)4-6(2)8-5/h3-4H,1-2H3

15513-52-7 Well-known Company Product Price

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  • (Code)Product description
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  • Aldrich

  • (532622)  3-Nitro-2,6-lutidine  97%

  • 15513-52-7

  • 532622-25G

  • 4,037.67CNY

  • Detail
  • Aldrich

  • (532622)  3-Nitro-2,6-lutidine  97%

  • 15513-52-7

  • 532622-25G

  • 4,037.67CNY

  • Detail
  • Aldrich

  • (532622)  3-Nitro-2,6-lutidine  97%

  • 15513-52-7

  • 532622-25G

  • 4,037.67CNY

  • Detail
  • Aldrich

  • (532622)  3-Nitro-2,6-lutidine  97%

  • 15513-52-7

  • 532622-25G

  • 4,037.67CNY

  • Detail

15513-52-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,6-Dimethyl-3-nitropyridine

1.2 Other means of identification

Product number -
Other names 2,5-DIMETHOXY-4-CHLOROPHENETHYLAMINE HYDROCHLORIDE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:15513-52-7 SDS

15513-52-7Relevant articles and documents

OXIDATIVE DEMETHYLATION OF SOME METHYLNITROPYRIDINE 1-OXIDES

Achremowicz, Lucjan

, p. 2433 - 2434 (1980)

3-Nitropyridine 1-oxide and 5-methyl-3-nitropyridine 1-oxide are produced readily by oxidative demethylation using SeO2 of 2-methyl- and 2,5-dimethyl-3-nitropyridine 1-oxides.

Silver(I)-Promoted ipso-Nitration of Carboxylic Acids by Nitronium Tetrafluoroborate

Natarajan, Palani,Chaudhary, Renu,Venugopalan, Paloth

, p. 10498 - 10504 (2015/11/18)

A novel and efficient method for the regioselective nitration of a series of aliphatic and aromatic carboxylic acids to their corresponding nitro compounds using nitronium tetrafluoroborate and silver carbonate in dimethylacetamide has been described. This transformation is believed to proceed via the alkyl-silver or aryl-silver intermediate, which subsequently reacts with the nitronium ion to form nitro substances. Mild reaction conditions, tolerant of a broad range of functional groups, and formation of only the ipso-nitrated products are the key features of this methodology when compared to known methods for syntheses of nitroalkyls and nitroarenes.

Nitration of Aromatic and Heteroaromatic Compounds by Dinitrogen Pentaoxide

Bakke, Jan M.,Hegbom, Ingrid,Oevreeide, Elin,Aaby, Kjersti

, p. 1001 - 1006 (2007/10/02)

Nitration of benzene and monosubstituted benzenes in liquid SO2 by dinitrogen pentaoxide at - 11 deg C gave the corresponding nitroarenes with substitution patterns similar to those obtained by nitrations with HNO3-H2SO4.For acetophenone an o/m ratio of 0.94 was obtained.The yields were dependent on the substituents.With a 1:1 ratio of arene: N2O5 the yields varied from 73percent for toluene to 0.4percent for nitrobenzene as substrates.From competition experiments and the nitration of bibenzyl it was concluded that the reaction was faster than the macroscopic rate of mixing.The qualitative order of reactivity for PhX was X = OCH3>CH3>H>Cl>CH3CO>NO2.Nitration with N2O5 in liquid CO2 gave similar results.Nitration of pyrimidine, pyrrole, imidazole and indole with N2O5-SO2 gave no nitrated products.With thiophene, 2- (34percent) and 3-nitrothiophene (5percent) together with 2,4-(16percent) and 2,5-dinitrothiophene (8percent) were obtained.With pyridine, mono- and di-methylpyridines, quinoline, isoquinoline and 4-phenylpyridine nitration of the pyridine ring was obtained.The yields varied from ca. 70percent to 16percent, except for 3,5-, 2,5- and 2,6-dimethylpyridine for which only traces of nitro-dimethylpyridines were obtained.The reaction with the pyridines appears to be intramolecular both in the SO2 phase and in the water phase used for quenching the reaction.The reaction was proposed to proceed by a complex formed in liquid SO2:

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