1601552-76-4Relevant academic research and scientific papers
Synthesis and characterization of novel unnatural di(8-daidzeinyl)methane
Xiao, Yong-Mei,Zhu, Xiao-Liang,Yuan, Jin-Wei,Yang, Liang-Ru,Xue, Ying,Mao, Pu,Qu, Ling-Bo
, p. 76 - 79 (2014)
A novel unnatural biflavonoid analog, di(8-daidzeinyl)methane, was synthesized using the C-C coupling reaction of daidzein and formaldehyde catalyzed by aliphatic amine in DMF, and its structure was characterized by ESI-MS, NMR, and FT-IR. Meanwhile, the effect parameters (catalyst, catalyst loading, temperature, and molar ratio of the substrates) were investigated and the optimized reaction conditions obtained using 9 mol % triethylamine as the catalyst, with the reaction run at 80°C for 20 h.
