16890-71-4Relevant academic research and scientific papers
THE REACTION OF NITROACETAMIDES WITH THIONATION REAGENTS SYNTHESIS OF MONO- AND DITHIO- OXALIC ACID DIAMIDES
Harris, Philip A.,Jackson, Arthur,Joule, John A.
, p. 3189 - 3192 (2007/10/02)
Nitroacetamides, R1(R2)N.CO.CH2NO2, react with phosphorus sulphide (P4S10) or 2,4-bis(4-methoxyphenyl)-1,2-dithiadiphosphetane-2,4-disulphide, Lawesson's reagent, to give amidethioamides, R1(R2)N.CO.CS.NH2.
Reactions of Cyanodithioformates with Primary Amines
Kibbel, H. U.,Kuecken, M.,Peters, E.,Weber, H.
, p. 41 - 48 (2007/10/02)
N-alkyldithiooxamides 3 and N,N-dialkyldithiooxamides 4 were synthesized in good yields by reaction of cyanodithioformates 1 with primary aliphatic amines.N-alkylcyanodithioformamides 2, intermediates in these reactions were obtained in very low yields only.The reaction of 1 and diaminoethane or 1,3-diaminopropane afforded imidazolidine-2-thione 5a respectively perhydropyrimidine-2-thione 5b.The reaction of 1 with 1-chloro-2-aminoethane did gave 2-thiocarbamoylthiazoline 7.
