201872-43-7Relevant academic research and scientific papers
N-3-oxoalkylamides and -thioamide in the synthesis of heterocyclic compounds. Part 1. Synthesis of 1,1-diethoxy-3-isothiocyanatobutane and reactions based on it
Fisyuk,Berdovich,Temnikov,Knyaz'kova
, p. 805 - 810 (1997)
The reaction of 3-isothiocyanatobutanal with ethanol in the presence of ethyl orthoformate produced 1,1-diethoxy-3-isothiocyanatobutane. The latter was used to devise methods of preparing 3-methylaminobutanal diethylacetal, N-(4-diethoxybutyl-2)thioamides
Synthesis of 3-isothiocyanatopropion-and-butyraldehyde diethyl acetals and their reactions with N-nucleophiles
Fisyuk,Mukanov
, p. 1269 - 1274 (2007/10/03)
A one-pot procedure was developed for the synthesis of 3- isothiocyanatopropionaldehyde and 3-isothiocyanatobutyraldehyde diethyl acetals from the corresponding α,β-unsaturated aldehydes. Reactions of 1,1-diethoxy-3-isothiocyanatobutane with aliphatic ami
