202277-52-9

Basic information

• Product Name: 4-(3-BROMO-PHENYL)-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER
• Synonyms: 4-(3-BROMO-PHENYL)-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER;Ethyl 4-(3-bromophenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
• CAS NO: 202277-52-9
• Molecular Formula: C₁₄H₁₅BrN₂O₃
• Molecular Weight: 339.18
• Mol File: 202277-52-9.mol
• Article Data: 66

Chemical Properties

• Boiling Point: 425.3°C at 760 mmHg
• Flash Point: 211°C
• Appearance: /
• Density: 1.42g/cm³
• Vapor Pressure: 1.94E-07mmHg at 25°C
• Refractive Index: 1.56
• CAS DataBase Reference: 4-(3-BROMO-PHENYL)-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER(CAS DataBase Reference)
• NIST Chemistry Reference: 4-(3-BROMO-PHENYL)-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER(202277-52-9)
• EPA Substance Registry System: 4-(3-BROMO-PHENYL)-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER(202277-52-9)

Safety Data

• Hazardous Substances Data: 202277-52-9(Hazardous Substances Data)

Usage

InChI:InChI=1/C14H15BrN2O3/c1-3-20-13(18)11-8(2)16-14(19)17-12(11)9-5-4-6-10(15)7-9/h4-7,12H,3H2,1-2H3,(H2,16,17,19)

Upstream product

• 3132-99-8 m-bromobenzoic aldehyde 
• 141-97-9 ethyl acetoacetate 
• 57-13-6 urea 
• 15852-73-0 (3-Bromophenyl)methanol 
• 75148-49-1 3-bromobenzaldehyde diethylacetal 
• 4433-85-6 2-ethyl-3-oxobutanoic acid 

Downstream Products

• 1159493-12-5 C₁₂H₁₃BrN₄O₂ 
• 1092074-28-6 ethyl 4-(3-bromophenyl)-1,2-dihydro-6-methyl-2-oxopyrimidine-5-carboxylate 

Relevant articles and documents

Fe3O4@mesoporous SBA-15: A robust and magnetically recoverable catalyst for one-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones via the Biginelli reaction

A magnetic nanoparticle conjugated mesoporous nanocatalyst (Fe 3O4@mesoporous SBA-15) with a high surface area has been synthesized by chemical conjugation of magnetite (Fe3O4) nanoparticles with functionalized

Magnetic Silica-Coated Picolylamine Copper Complex [Fe3O4@SiO2@GP/Picolylamine-Cu(II)]-Catalyzed Biginelli Annulation Reaction

An efficient and heterogeneous novel magnetic silica-coated picolylaminecopper complex [Fe3O4@SiO2@GP/Picolylamine-Cu(II)] was synthesized, characterized, and employed as a magnetically recoverable nanocatalyst in Biginelli condensation for the preparatio

Tungsten-substituted molybdophosphoric acid impregnated with kaolin: effective catalysts for the synthesis of 3,4-dihydropyrimidin-2(1: H)-ones v i a biginelli reaction

A series of highly reusable heterogeneous catalysts (10-25 wt% PMo7W5/kaolin), consisting of tungsten-substituted molybdophosphoric acid, H3PMo7W5O40·24H2O (PMo7W5) impregnated with acid treated kaolin clay was synthesized by the wetness impregnation meth

1, 1'-sulfinyldiethylammonium bis (hydrogen sulfate) as a recyclable dicationic ionic liquid catalyst for the efficient solvent-free synthesis of 3, 4-dihydropyrimidin-2(1H)-ones Via biginelli reaction

Objective: A facile and efficient method for synthesis of 3, 4-dihydropyrimidin-2(1H)-ones via Biginelli reaction catalyzed by a novel dicationic Br?nsted acidic ionic liquid, [(EtNH2)2SO][HSO4]2, has been succe