22760-66-3

Basic information

• Product Name: Butanamide, 2-diazo-3-oxo-N-phenyl-
• CAS NO: 22760-66-3
• Molecular Formula: C10H9N3O2
• Molecular Weight: 203.2
• Mol File: 22760-66-3.mol
• Article Data: 5

Chemical Properties

• CAS DataBase Reference: Butanamide, 2-diazo-3-oxo-N-phenyl-(CAS DataBase Reference)
• NIST Chemistry Reference: Butanamide, 2-diazo-3-oxo-N-phenyl-(22760-66-3)
• EPA Substance Registry System: Butanamide, 2-diazo-3-oxo-N-phenyl-(22760-66-3)

Safety Data

• Hazardous Substances Data: 22760-66-3(Hazardous Substances Data)

Upstream product

• 674-82-8 4-methyleneoxetan-2-one 
• 62-53-3 aniline 
• 87742-62-9 (Z)-3-Hydroxy-but-2-enoic acid phenylamide 
• 102-01-2 N-phenylacetoacetamide 
• 32113-04-5 4-azido-2-methylquinoline 
• 74227-77-3 4-azido-7-(trifluoromethyl)quinoline 
• 69063-03-2 4-azido-7-chloro-quinoline 
• 149848-27-1 4-Azido-7-chloro-2-methyl-quinoline 
• 149848-16-8 4-Azido-6-cyclohexyl-quinoline 
• 149848-23-7 4-Azido-6-cyclohexyl-2-methyl-quinoline 
• 149848-24-8 8-Azido-6-methyl-[1,3]dioxolo[4,5-g]quinoline 
• 149848-26-0 4-azido-8-trifluoromethylquinoline 
• 149848-31-7 8-Azido-6-phenyl-[1,3]dioxolo[4,5-g]quinoline 

Downstream Products

• 18649-98-4 dimethylsulfonium 2-oxo-1-<(phenylamino)carbonyl>propylide 
• 1421852-09-6 2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-1-(prop-2-yn-1-yl)-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-08-5 1-allyl-2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-07-4 1-cyclopropyl-2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-06-3 1-butyl-2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-04-1 1-(4-methoxyphenyl)-2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-02-9 2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-1-(p-tolyl)-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-00-7 2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-1-(m-tolyl)-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1421852-10-9 2,5-dimethyl-3-oxo-N²,N⁴-diphenyl-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1002555-88-5 2,5-dimethyl-3-oxo-N²,N⁴,1-triphenyl-2,3-dihydro-1H-pyrrole-2,4-dicarboxamide 
• 1384290-55-4 5-methyl-N-phenyl-1-(prop-2-yn-1-yl)-1H-1,2,3-triazole-4-carboxamide 
• 1205041-55-9 1-benzyl-5-methyl-N-phenyl-1H-1,2,3-triazole-4-carboxamide 
• 892299-32-0 5-methyl-N-phenyl-1-(o-tolyl)-1H-1,2,3-triazole-4-carboxamide 
• 1384290-49-6 1-cyclopropyl-5-methyl-N-phenyl-1H-1,2,3-triazole-4-carboxamide 

Relevant articles and documents

Copper-catalyzed chemoselective cross-coupling reaction of thioamides and α-diazocarbonyl compounds: Synthesis of enaminones

The development of operationally simple and cost-effective methods for C[sbnd]C bond formation reactions are highly important in pharmaceutical, agrochemical and material research. In this article we describe the first copper-catalyzed cross-coupling reaction of thioamides with acceptor/acceptor-substituted and acceptor-only substituted α-diazocarbonyl compounds to yield enaminones. The reaction shows broad substrate scope in terms of thioamides and diazocarbonyl compounds. Primary, secondary and tertiary thioamides all give enanminones when reacted with α-diazodiesters, α-diazoketoesters, α-diazodiketones, α-diazoketoamides, α-diazoesteramides, α-diazoketosulfones and α-diazomonoketones.

New 1-[quinolyl(4)]-1,2,3-triazoles: Synthesis and evaluation of antiinflammatory and analgesic properties. III

Several 1-[quinolyl(4)]-1,2,3-triazoles were synthesized by 1,3-dipolar cycloaddition of 4-azidoquinolines with activated methylene compounds. The synthesized compounds, tested for antiinflammatory and analgesic activities, resulted moderately active as antiinflammatories, but with a very interesting analgesic activity, sometimes higher than that of indomethacin, used as reference drug. Some of the triazole derivatives were evaluated also as antimicrobial, but none of them exhibited activity.

Preparation of 3-Acetyl-2-hydroxyindoles via Rhodium Carbenoid Aromatic C-H Insertion

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