23358-95-4Relevant articles and documents
Preparation method and separation method of low polymerization cyclic polymer
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Paragraph 0187-0235, (2019/11/20)
The invention provides a preparation method of a low polymerization cyclic polymer, and the method comprises the following steps: (1-1) in an organic solvent A, terephthaloyl chloride and 1,4-butanediol undergo esterification reaction under the action of
A practical synthesis of the cyclic butylene terephthalate trimer
Li, Xiaolin,Zhou, Pu,Wu, Wenxuan,Zhan, Li,Liu, Ting,Yang, Fan,Tang, Jie,Yu, Shanbao,Li, Hui,Luo, Yu
, p. 483 - 490 (2018/03/27)
This paper described a practical synthetic approach for the cyclic butylene terephthalate trimer (7). The key step was a ring-closing metathesis, using Grubbs' second-generation catalyst to form the macrocyclic ring. The advantages of this procedure included short reaction steps, simple operations and good yields.
Polybutylene terephthalate cyclic trimerization preparation of (by machine translation)
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Paragraph 0046; 0047; 0048, (2018/01/19)
The invention specifically has described a kind of new cyclic trimeric butylene terephthalate (Cyclic PBT Dimer) method for preparing, in the terephthalic chloride and 1, the 4 the protecting [...] butanediol as raw material with oriented synthesis strategy of deprotection of the polybutylene terephthalate cyclic trimerization, in the plastics can be used for the PBT polybutylene terephthalate cyclic trimerization contrast analysis of the impurity with the detection. Said product of this invention the chemical structural formula is: (by machine translation)