264147-43-5Relevant academic research and scientific papers
A short and facile synthesis of 2-(1Z)-(3-hydroxy-3,7-dimethylocta-1,6- dienyl)-1,4-benzenediol and 1-(3′-methoxypropanoyl)-2,4,5- trimethoxybenzene isolated from Cordia alliodora
Kaur, Sukhbir,Singh, Vasundhara,Kumar, Gulshan,Kad,Singh, Jasvinder
experimental part, p. 440 - 447 (2010/09/20)
A novel synthesis of 2-(1Z)-(3-hydroxy-3,7-dimethylocta-1,6-dienyl)-1,4- benzenediol and 1-(3′-methoxypropanoyl)-2,4,5-trimethoxybenzene has been carried out by making use of an easily available starting material, acceleration by MW irradiation and the use of water as a green solvent in the key steps.
Solid-supported green synthesis of substituted hydrocinnamic esters by focused microwave irradiation
Kumar, Vinod,Sharma, Anuj,Sinha, Arun K.
, p. 483 - 495 (2007/10/03)
An efficient chemoselective hydrogenation protocol for substituted cinnamic esters is developed for the synthesis in quantitative yield of corresponding bioactive dihydrocinnamic esters with solid-supported palladium chloride/ammonium formate (cat.) in HCOOH/H2O 1:2 as a hydrogenating agent under focused-microwave irradiation for 10 min.
Friedel-crafts reaction of activated benzene rings with captodative and electron-deficient alkenes. A one-step synthesis of the natural product methyl 3-(2,4,5-trimethoxyphenyl)propionate
Aguilar, Raul,Benavides, Adriana,Tamariz, Joaquin
, p. 2719 - 2735 (2007/10/03)
Electrophilic aromatic substitution of activated benzenes with the captodative olefin 1-acetylvinyl-1-p-nitrobenzoate (9), and with the electron-deficient alkenes methyl acrylate (8a), methylvinylketone (8b), and acrolein (8c) were evaluated under Lewis a
A concise conversion of β-asarone into 1-(3′- methoxypropanoyl)-2,4,5-trimethoxybenzene occurring in Cordia alliodora
Sinha, Arun K.,Dogra, Ruchi,Joshi, Bhupendra P.
, p. 635 - 638 (2007/10/03)
The first synthesis of 1-(3′-methoxypropanoyl)-2,4,5- trimethoxybenzene 4, a natural phenylpropanoid occurring in Cordia alliodora, has been achieved, from β-asarone 1 of Acorus calamus. Selenium dioxide oxidation of 1 leads to 2,4,5-trimethoxycinnamaldeh
