2812-74-0Relevant academic research and scientific papers
Synthesis of O-Alkyl Carbonochloridothioates
Martinez, Manuel A.,Vega, Juan C.
, p. 760 - 761 (1986)
The preparation of O-alkyl carbonochloridothioates (2) was improved by performing the reaction of thiophosgene with potassium alkoxides in the corresponding alcohol or in tetrahydrofuran at -65 deg C for 1 hour.In all cases, the reaction yielded products 2, O,O-dialkyl carbonothioates (4), and dialkyl carbonates (5) in varying distribution.
