Synthesis p. 760 - 761 (1986)
Update date:2022-08-02
Topics:
Martinez, Manuel A.
Vega, Juan C.
The preparation of O-alkyl carbonochloridothioates (2) was improved by performing the reaction of thiophosgene with potassium alkoxides in the corresponding alcohol or in tetrahydrofuran at -65 deg C for 1 hour.In all cases, the reaction yielded products 2, O,O-dialkyl carbonothioates (4), and dialkyl carbonates (5) in varying distribution.
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(1988)Doi:10.1016/j.saa.2009.01.019
(2009)
