2813-23-2

Basic information

• Product Name: 4'-Methoxy-2-(methylsulfinyl)acetophenone
• Synonyms: 4'-Methoxy-2-(methylsulfinyl)acetophenone;4'-Methoxy-α-(methylsulfinyl)acetophenone;Methyl(2-oxo-2-(4-methoxyphenyl)ethyl) sulfoxide
• CAS NO: 2813-23-2
• Molecular Formula: C₁₀H₁₂O₃S
• Molecular Weight: 0
• Mol File: 2813-23-2.mol
• Article Data: 2

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 4'-Methoxy-2-(methylsulfinyl)acetophenone(CAS DataBase Reference)
• NIST Chemistry Reference: 4'-Methoxy-2-(methylsulfinyl)acetophenone(2813-23-2)
• EPA Substance Registry System: 4'-Methoxy-2-(methylsulfinyl)acetophenone(2813-23-2)

Safety Data

• Hazardous Substances Data: 2813-23-2(Hazardous Substances Data)

Upstream product

• 100-07-2 4-methoxy-benzoyl chloride 
• 67-68-5 dimethyl sulfoxide 
• 94-30-4 ethyl 4-methoxybenzoate 
• 123-11-5 4-methoxy-benzaldehyde 
• 13350-29-3 1-Hydroxy-1-(4-methoxy-phenyl)-aethan-methyl-sulfoxid 

Downstream Products

• 86988-54-7 2-(4-methoxyphenyl)pyrido<3,4-b>pyrazine 
• 61161-13-5 4'-methoxy-2,2-bis(p-methoxyphenyl)acetophenone 
• 1361298-17-0 N-(2,5-dimethoxyphenyl)-2-(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-amine 
• 1361298-36-3 8-amino-2-(4-methoxyphenyl)pyrido[3,4-b]pyrazine 
• 1361298-31-8 N-[2-(4-methoxyphenyl)pyrido[3,4-b]pyrazin-8-yl]benzophenone imine 
• 1361298-24-9 8-bromo-2-(4-methoxyphenyl)pyrido[3,4-b]pyrazine 
• 60112-43-8 (E)-methyl 4-hydroxy-4-(4-methoxyphenyl)-but-2-enoate 
• 32149-29-4 4-(4-methoxy-phenyl)-4-oxo-but-2-enoic acid methyl ester 
• 152423-69-3 1-(4-Methoxy-phenyl)-2,2,2-tris-methylsulfanyl-ethanone 
• 87228-61-3 S-methyl 2-(4-methoxyphenyl)-2-oxoethanethioate 
• 13603-51-5 2-hydroxy-1-(4-methoxyphenyl)-2-(methylsulfanyl)ethan-1-one 
• 100749-29-9 2-Methanesulfinyl-1,5-bis-(4-methoxy-phenyl)-pentane-1,5-dione 
• 122033-80-1 ω-(Methylthio)-ω-(methylsulfinyl)-p-methoxyacetophenone 
• 52109-55-4 N-[2-(4-Methoxy-phenyl)-1-methylsulfanyl-2-oxo-ethyl]-benzamide 

Relevant articles and documents

Preparation method of beta-ketosulfoxide based on CaC2 catalysis

The invention provides a preparation method of beta-ketosulfoxide based on CaC2 catalysis, and belongs to the technical field of organic synthesis. In the presence of CaC2 or NaH or in the co-presence of CaC2 and TEA, acyl chloride and dimethyl sulfoxide react to prepare the beta-ketosulfoxide compound, the yield of beta-ketosulfoxide is 8.7-78%, and the yield of beta-ketosulfoxide in the reaction process of acyl chloride and dimethyl sulfoxide is remarkably improved. Particularly, in the coexistence of CaC2 and TEA, acyl chloride and dimethyl sulfoxide react to prepare the beta-ketosulfoxide compound, the yield of beta-ketosulfoxide is 45-78%, and the preparation method is green, environmentally friendly, mild in reaction process and simple to operate.