32954-43-1Relevant articles and documents
A lycine amphoteric surface active agent and its preparation method
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Paragraph 0051; 0054; 0066; 0070; 0074; 0078, (2018/10/02)
The invention discloses a glycine betaine-type ampholytic surfactant and a preparation method thereof. The preparation method of the glycine betaine-type ampholytic surfactant comprises the following steps of (1) amidation reaction: carrying out amidation reaction on natural fatty acid and 3-dimethylaminopropylamine under the action of a catalyst, and timely removing water generated through reaction by using a 4A molecular sieve to obtain alkylamid-propyl dimethyl tertiary amine; and (2) quaterisation reaction: carrying out quaterisation reaction on alkylamid-propyl dimethyl tertiary amine and sodium chloroacetate in a solvent to obtain the glycine betaine-type ampholytic surfactant. The ampholytic surfactant group contains an amido bond, the performance of the molecule is changed, the glycine betaine-type ampholytic surfactant has better foam stability and mild performance, and the emulsifiability is obviously superior to that of the glycine betaine-type ampholytic surfactant. The preparation method is simple in process and low in production cost; the raw materials are green and natural; the water generated in the amidation reaction process is absorbed through the 4A molecular sieve; and the yield is improved.