33647-67-5

Basic information

• Product Name: DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL
• Synonyms: DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL;dl-2,5-dihydro-2,5-dimethoxy-alpha-methyl-2-furanmethanol;DL-1-(2,5-Dimethoxy-2,5-dihydrofuran-2-yl)ethanol,98%
• CAS NO: 33647-67-5
• Molecular Formula: C₈H₁₄O₄
• Molecular Weight: 174.19
• Mol File: 33647-67-5.mol
• Article Data: 8

Chemical Properties

• Boiling Point: 64-68 °C (1 mmHg)
• Flash Point: 111.6°C
• Appearance: /
• Density: 1.1699 (rough estimate)
• Vapor Pressure: 0.00171mmHg at 25°C
• Refractive Index: 1.4455 (estimate)
• Storage Temp.: 0-6°C
• CAS DataBase Reference: DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL(CAS DataBase Reference)
• NIST Chemistry Reference: DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL(33647-67-5)
• EPA Substance Registry System: DL-1-(2,5-DIMETHOXY-2,5-DIHYDROFURAN-2-YL)ETHANOL(33647-67-5)

Safety Data

• Safety Statements: 24/25
• Hazardous Substances Data: 33647-67-5(Hazardous Substances Data)

Usage

InChI:InChI=1/C8H14O4/c1-6(9)8(11-3)5-4-7(10-2)12-8/h4-7,9H,1-3H3/t6-,7-,8-/m1/s1

Upstream product

• 1192-62-7 1-(2-furyl)-1-ethanone 
• 67-56-1 methanol 
• 4208-64-4 (S)-1-(2-furanyl)ethanol 
• 4208-64-4 1-(2-furyl)ethanol 
• 113531-28-5 Octanoic acid 1-furan-2-yl-ethyl ester 
• 13129-26-5 1-(3'-furyl)-ethanol 

Downstream Products

• 34385-27-8 methyl 4-O-benzoyl-2,3,6-trideoxy-α-DL-threo-hex-2-enopyranoside 
• 18977-92-9 methyl α-DL-ristosaminide 
• 18977-92-9 methyl α-DL-daunosaminide 
• 6605-27-2 methyl 3-acetamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside 
• 6605-26-1 N,O-diacetyl-α-daunosaminide 
• 17016-64-7 methyl 3-benzamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside 
• 18977-93-0 3-amino-2,3,6-trideoxy-DL-lyxo-hexopyranoside hydrochloride 
• 32385-06-1 (+/-)-Ristosamine methyl ether 
• 62774-42-9 methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside 
• 97327-50-9 methyl 4-O-(N-benzoylbenzimidoyl)-2,3,6-trideoxy-α-DL-threo-hex-2-enopyranoside 
• 97327-52-1 methyl 3-benzamido-4-O-benzoyl-2-bromo-2,3,6-trideoxy-α-DL-galactopyranoside 
• 4208-64-4 1-(2-furyl)ethanol 
• 5158-60-1 methyl 6-deoxy-3-O-methyl-α-L-mannopyranoside 
• 1192-62-7 1-(2-furyl)-1-ethanone 

Relevant articles and documents

Asymmetric synthesis of methyl 6-deoxy-3-O-methyl-α-l-mannopyranoside from a non-carbohydrate precursor

A novel method is reported for preparing methyl 6-deoxy-3-O-methyl-α- l-mannopyranoside (1) by asymmetric synthesis, using 2-acetylfuran (2), a non-chiral simple molecule, as the starting material and achieving high yields via (S)-1-(2-furyl)ethanol and (

Electroorganic synthesis of 2,5-dialkoxydihydrofurans and pyridazines on solid phase using polymer beads as supports

Electroorganic synthesis has defied application in Solid-Phase Organic Synthesis (SPOS) so far. Typically more than 99.9% of the substrate molecules immobilized on a polymeric support are buried in the interior of the bead, and therefore are unable to undergo direct contact with a heterogeneous reagent such as an electrode. This intrinsic impediment for an electrochemical reaction can be overcome by the use of a redox mediator which shuttles electrons from the electrode to the polymer bound substrate molecules. This approach of indirect electroorganic synthesis was successfully applied for the 2,5-dialkoxylation of furans on solid phase. The oxidation products can be hydrolyzed and through condensation with hydrazine hydrate substituted pyridazines are produced in 50-65% overall yield. Georg Thieme Verlag Stuttgart.

Synthesis of 1-(2,5-dimethoxy-2,5-dihydrofuran-2-yl)ethanol from 2-acetylfuran

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