4073-59-0Relevant articles and documents
A convenient method for the preparation of functionalized N-acylsulfenamides from primary amides
Musiejuk, Mateusz,Witt, Dariusz
supporting information, p. 305 - 310 (2016/02/18)
We have developed a convenient method for the synthesis of functionalized N-acylsulfenamides under mild conditions and in moderate to good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)-disulfanyl derivatives with nitrogen nucleophiles generated from primary amides or imides and sodium hydride. The developed method allows for the preparation of N-acylsulfenamides bearing additional hydroxyl, carboxyl, or amino functionalities.
TBAF promoted formation of symmetrical trisulfides
Lach, Slawomir,Witt, Dariusz
, p. 10 - 14 (2014/02/14)
We have developed a new method for the synthesis of functionalized symmetrical trisulfides based on (5,5-dimethyl-2-thioxo-1,3,2-dioxa-phosphorin- 2-yl)disulfanyl derivatives prepared from readily available 5,5-dimethyl-2-sul- fanyl-2-thioxo-1,3,2-dioxaph
An efficient and convenient synthesis of unsymmetrical disulfides from thioacetates
Lach, Slawomir,Demkowicz, Sebastian,Witt, Dariusz
supporting information, p. 7021 - 7023 (2013/12/04)
We have developed convenient methods for the synthesis of functionalized unsymmetrical dialkyl disulfides under mild conditions in very good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2- dioxaphosphorinan-2-yl)-disu