51898-34-1Relevant articles and documents
Synthesis method of tocopherol nicotinate
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Paragraph 0008; 0016; 0018-0033, (2021/10/30)
The invention belongs to the technical field of organic chemical synthesis, and relates to a method for preparing tocopherol nicotinate from 3-pyridylaldehyde and tocopherol. According to the method, 3-pyridylaldehyde and tocopherol are used as raw materials, N-heterocyclic carbene is used as a catalyst, and tocopherol nicotinate is synthesized through oxidative esterification. The method has the advantages of cheap raw materials, mild reaction conditions, simple process, greenness, safety, high efficiency and environmental protection, and is suitable for industrial production.
One-pot preparation of esters from carboxylic acids using the PPh3-CCl3CN system
Jang, Doo Ok,Cho, Dae Hyan,Kim, Joong-Gon
, p. 2885 - 2890 (2007/10/03)
A convenient one-pot process for preparing various esters from carboxylic acids using the Ph3P-CCl3CN has been developed. Racemic α-tocopherol, clofibrate and flavoxate were prepared in high yields using this method.
N,N-BIS(2-OXO-3-OXAZOLIDINYL)PHOSPHORDIAMIDIC CHLORIDE (CLSPO): A NEW STRATEGY FOR THE ESTER FUNCTION PREPARATION
Ballester-Rodes, M.,Palomo-Coll, A. L.
, p. 515 - 520 (2007/10/02)
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