578-85-8Relevant articles and documents
Preparation method of dye intermediate 1-naphthol-3,6-disulfonic acid (RG acid)
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Paragraph 0038; 0039; 0040, (2016/11/17)
The invention relates to the field of organic synthesis, and relates to a preparation method of a dye intermediate 1-naphthol-3,6-disulfonic acid (RG acid). According to the invention, an industrial product 2,7-naphthalene disulfonic acid is adopted as an initial material; and 1-naphthol-3,6-disulfonic acid (RG acid) with a single component and with purity reaching 98% or higher is obtained through three steps of reactions which are nitration, reduction and hydrolysis. During the preparation process provided by the invention, no waste gas and waste solid is emitted. Mother liquor produced through nitration and hydrolysis is subjected to a concentration treatment. Concentrate liquid and evaporated water can be returned to the reaction, and substantially no wastewater is discharged during the entire process. The process has the advantages of simple operation process, mild reaction conditions, and good product quality. The method provided by the invention is a novel route suitable for RG acid industrial production.
Aromatic azo sulfonylnitrene compounds
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, (2008/06/13)
Compounds of the structure SPC1 Wherein R and R1 are the same or different and are selected from the group consisting of hydrogen, halogen, and alkyl from one to four carbon atoms, inclusive, and R2 is a substance which inhibits thrombogenic or clotting activity of a material and is that portion of a substituted aromatic which couples with a diazonium salt.