92-41-1Relevant articles and documents
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Lynch,Scanlan
, (1927)
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Environmental-friendly H-acid synthesis method
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Paragraph 0036-0038, (2017/10/13)
The invention relates to a synthesis method and in particular relates to an environmental-friendly H-acid synthesis method which comprises the following steps: performing disulfonic treatment, performing bromination treatment, performing nitration treatment, and separating a middle body, namely 1-bromine-8-nitro-3,6-naphthalene disulfonic acid. The environmental-friendly H-acid synthesis method is capable of reducing environment pollution and preventing such potential safety hazard, and thus an operation environment is relatively safe and environmentally friendly.
Process for separation of naphthalenedisulfonic acids
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, (2008/06/13)
A process for separating 1,6-naphthalenedisulfonic acid, 2,6-naphthalenedisulfonic acid or 2,7-naphthalenedisulfonic acid selectively from reaction mixtures obtained by disulfonation of naphthalene under different reaction conditions is disclosed. For example, a particular disulfonation reaction of naphthalene is carried out which favors the formation of a particular isomer. This reaction mixture is diluted with water to adjust the sulfuric acid concentration to 35 to 90% by weight and the temperature is maintained at 0° to 80° C.; 1,6-naphthalene-disulfonic acid is selectively separated at high purity.