57880-71-4Relevant articles and documents
3,3-Dichloro-4-(p-methoxyphenyl)-1-phenyl-2-azetidinone
Ercan,Ulku,Guner
, p. 1779 - 1780 (1996)
The structure of the title compound consists of discrete C16H13Cl2NO2 molecules with a closest intermolecular contact of 2.54 (3) angstroms between the carbonyl O atom and a methyl H atom. The four-membered ring is nearly planar, with long C-C distances of 1.564 (5) and 1.537 (5) angstroms, similar to the distances observed in other substituted monocyclic β-lactams. The dihedral angle between the planes of the phenyl rings is 78.6 (1)°.
Reaction of Imines with Trichloroacetic Esters or Anhydride Promoted by Iron Carbonyl or Microwave Irradiation. Preparation of 3,3-Dichloro-β-Lactams
Khajavi, Mohammad S.,Sefidkon, Fatemeh,Sadat Hosseini
, p. 724 - 725 (2007/10/03)
The synthesis of 3,3-dichloroazetidin-2-ones by the reaction of imines and methyl or trimethylsilyl trichloroacetate promoted by diiron nonacarbonyl or by microwave irradiation of imines and trichloroacetic anhydride is described.