64096-86-2Relevant articles and documents
NEW PROCESS FOR THE PREPARATION OF AMENAMEVIR
-
Page/Page column 5-6, (2020/12/30)
The present invention relates to an improved process for the preparation of Amenamevir and derivatives thereof via a four component Ugi reaction.
A practical, efficient synthesis of 1,1-dioxo-hexahydro-1#-thiopyran-4- carbaldehyde
Bio, Matthew M.,Hansen, Karl B.,Gipson, John
, p. 892 - 895 (2013/01/03)
A practical, efficient, and scalable procedure for the preparation of l,1-dioxo-hexahydro-1λ6-thiopyran-4-carbaldehyde is reported. Synthesis of this aldehyde was complicated by high aqueous solubility of the product and the intermediates. The isolation and purification of the aldehyde was accomplished by conversion to the crystalline bisulfite adduct.