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65527-61-9

65527-61-9

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65527-61-9 Usage

Uses

N-Allylnorylsergic Acid N,N-Diethylamide acts as a D1 dopamine receptor antagonist due to its analagous structure to LSD.

Check Digit Verification of cas no

The CAS Registry Mumber 65527-61-9 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 6,5,5,2 and 7 respectively; the second part has 2 digits, 6 and 1 respectively.
Calculate Digit Verification of CAS Registry Number 65527-61:
(7*6)+(6*5)+(5*5)+(4*2)+(3*7)+(2*6)+(1*1)=139
139 % 10 = 9
So 65527-61-9 is a valid CAS Registry Number.

65527-61-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 13, 2017

Revision Date: Aug 13, 2017

1.Identification

1.1 GHS Product identifier

Product name (6aR,9R)-N,N-diethyl-7-prop-2-enyl-6,6a,8,9-tetrahydro-4H-indolo[4,3-fg]quinoline-9-carboxamide

1.2 Other means of identification

Product number -
Other names 6-Allyl-6-nor-lysergic acid diethylamide

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:65527-61-9 SDS

65527-61-9Synthetic route

allyl bromide
106-95-6

allyl bromide

8β-6-norlysergic acid diethylamide
35779-43-2

8β-6-norlysergic acid diethylamide

N-AllylnorLSD
65527-61-9

N-AllylnorLSD

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 0.5h;88%
allyl bromide
106-95-6

allyl bromide

6-norlysergic acid diethylamide
35779-43-2, 71953-76-9

6-norlysergic acid diethylamide

A

N-AllylnorLSD
65527-61-9

N-AllylnorLSD

B

(6aR,9S)-7-Allyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

(6aR,9S)-7-Allyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinoline-9-carboxylic acid diethylamide

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h;A 0.050 g
B 0.039 g
9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide
35779-41-0

9,10-didehydro-N,N-diethyl-6-cyanoergoline-8β-carboxamide

N-AllylnorLSD
65527-61-9

N-AllylnorLSD

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 61 percent / Zn / acetic acid; H2O / 4 h / Heating
2: 88 percent / K2CO3 / dimethylformamide / 0.5 h / 25 °C
View Scheme
lysergide
50-37-3

lysergide

N-AllylnorLSD
65527-61-9

N-AllylnorLSD

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 71 percent / CCl4; CHCl3 / 6 h / Heating
2: 61 percent / Zn / acetic acid; H2O / 4 h / Heating
3: 88 percent / K2CO3 / dimethylformamide / 0.5 h / 25 °C
View Scheme

65527-61-9Downstream Products

65527-61-9Relevant articles and documents

Stereochemical and NMR Reassignment of 6-Norlysergic Acid Diethylamide and 6-Nor-6-allyllysergic Acid Diethylamide

Stachulski, Andrew V.,Nichols, David E.,Scheinmann, Feodor

, p. 30 - 31 (2007/10/03)

Conditions are described for the preparation of a salt of 8β-norlysergic acid diethylamide (8β-nor-LSD) 1 as a single epimer from cyanamide 3, whereas earlier preparations gave mixtures of 1 with the 8α epimer 4 in variable proportions: the earlier NMR assignment of 1 is amended and the N(6) alkylation of 1 and 4 with allyl bromide is discussed.

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