71357-60-3

Basic information

• Product Name: 2-Cyclohexen-1-ol, 4-(3,4-dimethoxyphenyl)-4-[2-(methylamino)ethyl]-, cis-
• CAS NO: 71357-60-3
• Molecular Formula: C17H25NO3
• Molecular Weight: 291.39
• Mol File: 71357-60-3.mol
• Article Data: 5

Chemical Properties

• CAS DataBase Reference: 2-Cyclohexen-1-ol, 4-(3,4-dimethoxyphenyl)-4-[2-(methylamino)ethyl]-, cis-(CAS DataBase Reference)
• NIST Chemistry Reference: 2-Cyclohexen-1-ol, 4-(3,4-dimethoxyphenyl)-4-[2-(methylamino)ethyl]-, cis-(71357-60-3)
• EPA Substance Registry System: 2-Cyclohexen-1-ol, 4-(3,4-dimethoxyphenyl)-4-[2-(methylamino)ethyl]-, cis-(71357-60-3)

Safety Data

• Hazardous Substances Data: 71357-60-3(Hazardous Substances Data)

Upstream product

• 593-51-1 methylamine hydrochloride 
• 86227-37-4 N-benzenesulfonyl 4-(3',4'-dimethoxyphenyl)-4-methylaminoethylcyclohex-2-en-1-one 
• 85753-65-7 N-[3-Cyano-3-(3,4-dimethoxy-phenyl)-propyl]-N-methyl-benzenesulfonamide 
• 86227-35-2 N-[3-(3,4-Dimethoxy-phenyl)-4-oxo-butyl]-N-methyl-benzenesulfonamide 
• 93-17-4 3,4-dimethoxyphenylacetonitrile 
• 87014-22-0 [1-(3,4-Dimethoxy-phenyl)-4-oxo-cyclohex-2-enyl]-acetic acid; compound with triethyl-amine 
• 87014-17-3 Acetic acid (1R,3S,6S)-6-(3,4-dimethoxy-phenyl)-8-oxo-bicyclo[4.2.0]oct-3-yl ester 
• 87014-23-1 [1-(3,4-Dimethoxy-phenyl)-4-oxo-cyclohex-2-enyl]-acetyl chloride 
• 87014-18-4 (3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one 
• 87014-19-5 (3aR,7aR)-3a-(3,4-Dimethoxy-phenyl)-hexahydro-benzofuran-2,6-dione 
• 70779-54-3 Acetic acid (7R,8S)-8-(3,4-dimethoxy-phenyl)-8-(2-oxo-ethyl)-1,4-dioxa-spiro[4.5]dec-7-yl ester 
• 70779-53-2 Acetic acid (7R,8S)-8-allyl-8-(3,4-dimethoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-7-yl ester 
• 121537-77-7 (1RS,2SR)-5,5-ethylenedioxy-2-(N-methylamidomethyl)-2-(3',4'-dimethoxyphenyl)cyclohexyl acetate 
• 121537-78-8 [(7R,8S)-7-Acetoxy-8-(3,4-dimethoxy-phenyl)-1,4-dioxa-spiro[4.5]dec-8-yl]-acetic acid methyl ester 

Downstream Products

• 71610-13-4 (+/-)-N,O-diacetyljoubertinamine 
• 71610-13-4 (+/-)-N,O-diacetyljoubertinamine 
• 468-53-1 (-)-mesembrine 

Relevant articles and documents

Total synthesis of (±)-joubertinamine from 3-(3,4-dimethoxyphenyl)- 5-bromo-2-pyrone

The regioselective synthesis and Diels-Alder cycloaddition of 3-(3,4-dimethoxyphenyl)-5-bromo-2-pyrone provided a new efficient synthetic route to joubertinamine (9.6% total yield over 10 steps).

A Synthesis of Seco-mesembrane Alkaloids, (+/-)-Joubertiamine, (+/-)-Joubertinamine, and (+/-)-Epijoubertinamine

A synthesis of seco-mesembrane alkaloids, (+/-)-joubertiamine (4), (+/-)-joubertinamine (5), and (+/-)-epijoubertinamine (6), was accomplished starting with 2-allyl-2-aryl-5,5-ethylenedioxycyclohexanones (10 and 3), which are readily available by allylati

SCELETIUM (AIZOACEAE) ALKALOIDS: TOTAL SYNTHESIS OF RACEMIC MESEMBRANONE, JOUBERTINAMINE AND EPIJOUBERTINAMINE

The total synthesis of the Sceletium alkaloids mesembranone, joubertinamine and epijoubertinamine via the intramolecular cyclization of an enone to a benzensulfonamide grouping under the conditions of a dissolving metal reduction is described.