82012-43-9Relevant academic research and scientific papers
New Methods and Reagents in Organic Synthesis. 20. 2-Mesitylenesulfonyl diazomethane: Synthesis and Application to the Arndt-Eistert Synthesis
Kuo, Ying-Che,Aoyama, Toyohiko,Shioiri, Takayuki
, p. 899 - 902 (2007/10/02)
2-Mesitylenesulfonyldiazomethane (4) was conveniently prepared from 2-mesitylenesulfonylchloride (5) in 4 steps.Reaction of 4 with benzoyl chloride smoothly furnished α-benzoyl α-(2-mesitylenesulfonyl)diazomethane (9).Thermal treatment of 9 in the presenc
