9004-77-7Relevant articles and documents
Preparation method of alkyl diglycol (by machine translation)
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Paragraph 0031-0044, (2020/06/09)
The invention relates to a preparation method of alkyl diglycol with NRE (narrow distribution ethoxylate Narrow Range Ethoxylate) effect while increasing the reaction speed in the presence of a novel aluminum-based catalyst containing alkali metal or alkaline earth metal. (by machine translation)
OPEN-FLASK HYDROBORATION AND THE USE THEREOF
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Paragraph 0046; 0058; 0059, (2018/03/25)
The present disclosure generally relates to a process for hydroboration of an alkene or alkyne using ammonia borane (AB). In particular, the present invention relates to hydroboration of an alkene or alkyne in the presence of air or moisture, and a clean process for facile preparation of an alcohol by oxidizing the organoborane so formed with hydrogen peroxide. The products, including aminodialkylboranes, ammonia trialkylborane complexes, as well as various alcohols so prepared, are within the scope of this disclosure.
Preparation method of ethylene glycol monobutyl ether
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Paragraph 0019; 0021, (2017/07/18)
The invention relates to the field of chemistry and chemical engineering and particularly discloses a preparation method of ethylene glycol monobutyl ether. The preparation method of the ethylene glycol monobutyl ether is characterized in that ethylene oxide and n-butyl alcohol are prepared into a raw material mixed solution, and cold storage is performed for usage; high-silicon-content alloy or an all-silicon molecular sieve and porous silicon dioxide are put in a muffle furnace to perform high-temperature roasting, and a roasting catalyst is put in a dryer for usage after being numbered; the raw material solution and the roasting catalyst are put in a reaction kettle for reaction, and a product is obtained. The high-silicon-content alloy or the all-silicon molecular sieve and the porous silicon dioxide used by the method is low in procurement cost, the treating process is simple, a production process is greatly simplified, the production cost is reduced, the catalyst or ethylene glycol butyl ether is high in selectivity, and the preparation method has very high stability.