9010-02-0Relevant articles and documents
Methods of producing glycidyl nitrate
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Page/Page column 14; 15, (2020/03/04)
Methods of producing glycidyl nitrate. The method comprises reacting glycerol and nitric acid in a microfluidic reactor to form a nitrated glycerol compound. The microfluidic reactor comprises a reaction volume of the microfluidic reactor of less than about 20 ml and an inner diameter of a reaction channel of the microfluidic reactor of less than or equal to about 1000 μm. The nitrated glycerol compound is reacted with a base in the microfluidic reactor to form glycidyl nitrate. Additional methods of producing glycidyl nitrate are also disclosed.
Continuous production nitroglycerin tablet (by machine translation)
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Paragraph 0070-0073, (2020/08/27)
To specific processes of continuous production of raw materials of nitroglycerin and continuous production of tablets, green, safe and no-risk synthesis is achieved in the continuous production of the green preparation of the nitroglycerin, and the combined API and the nitroglycerin tablet are integrated. (by machine translation)
Low hazard small-scale synthesis and chemical analysis of high purity nitroglycerine (NG)
Contini, Alessandro E.,Flood, Nathan,McAteer, Daniel,Mai, Nathalie,Akhavan, Jacqueline
, p. 87228 - 87232 (2015/11/09)
A previously reported two-phase (99.5% fuming nitric acid/dichloromethane) batch method to prepare high purity 1,2,3-propanetriyl trinitrate (nitroglycerine, NG) was evaluated, simplified and adapted specifically for low hazard small-scale synthesis. The purity of the product, as determined by NMR spectroscopy, HPLC and IR spectroscopic analysis was found to be greater than 99%. The quick synthetic method is highly recommended when small amounts of highly pure NG are required for analytical and related purposes in the absence of a microreactor.