91061-33-5Relevant academic research and scientific papers
A process for preparing 2 - [4 - (2 - ethoxy-ethyl) - 2, 3 - dimethyl-phenoxy] trifluoroethylamine (by machine translation)
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, (2018/09/13)
The invention discloses a process for preparing 2 - [4 - (2 - ethoxy-ethyl) - 2, 3 - dimethyl-phenoxy] trifluoroethylamine, belongs to the technical field of organic chemistry. In order to 2, 3 - dimethyl phenol as raw material passes through 1 step react
Method for preparing 2-[4-(2-ethoxyethyl)phenoxy]ethylamine
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, (2018/11/22)
The invention discloses a method for preparing 2-[4-(2-ethoxyethyl)phenoxy]ethylamine and belongs to the technical field of organic chemistry. The method comprises the steps: (1) subjecting phenol, which serves as a raw material, to chloracetylation; (2)
Direct Synthesis of α-Alkoxy Ketones by Oxidative C–O Bond Formation
Yu, Hui,Xu, Yilan,Fang, Yan,Dong, Rui
, p. 5257 - 5262 (2016/11/13)
A convenient method to prepare α-alkoxy ketones has been developed by oxidative coupling of aryl methyl ketones and alcohols. With aqueous tert-butyl hydroperoxide (6.0 equiv.) as the oxidant, tetrabutylammonium iodide (20 mol-%) as the catalyst, and TsNHNH2(1.0 equiv.) as the additive, ketones underwent direct alkoxylation to give α-methoxy or α-ethoxy ketones in moderate to good yields.
Efficient synthesis of resin-bound α-TMSdiazoketones and their use in solid-phase organic synthesis
Iso, Yasuyoshi,Shindo, Hirohisa,Hamana, Hiroshi
, p. 5353 - 5361 (2007/10/03)
α-TMSdiazoketones on a solid support could be simply and efficiently prepared by reaction of the corresponding resin-bound acid chlorides with excess TMSdiazomethane, without any bases. These α-TMSdiazoketones were used via carbenes or carbenoids for a variety of solid-phase reactions. These useful solid-phase reactions allow efficient construction of diverse compound libraries by use of combinatorial chemistry, due to the high reactivity and wide applications of the carbenes or carbenoids. (C) 2000 Elsevier Science Ltd.
