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Cas Database |
| Name |
1,1,2,3-Tetrachloropropene |
EINECS | N/A |
| CAS No. | 10436-39-2 | Density | 1.539g/cm3 |
| PSA | 0.00000 | LogP | 3.11070 |
| Solubility | MISCIBLE | Melting Point |
29-31°C(lit.) |
| Formula | C3H2 Cl4 | Boiling Point | 173.8°Cat760mmHg |
| Molecular Weight | 179.861 | Flash Point | 62.3°C |
| Transport Information | N/A | Appearance | clear colorless to yellowish liquid after melting |
| Safety | Poison by ingestion and skin contact. Moderately toxic by inhalation. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of Cl−. See also CHLORINATED HYDROCARBONS, ALIPHATIC. | Risk Codes | R37/38; R41; R36/37/38; R34 |
| Molecular Structure |
|
Hazard Symbols |
 Xi, C
|
| Synonyms |
Propene,1,1,2,3-tetrachloro- (6CI,7CI,8CI); 1,1,2,3-Tetrachloro-1-propene;1,1,2,3-Tetrachloropropene; 2,3,3-Trichloroallyl chloride; HCO 1230; HCO 1230xa |
Article Data | 33 |
1,1,2,3-Tetrachloropropene Synthetic route
- 16714-68-4
1,1,2,2,3-pentachloropropane
- 10436-39-2
1,1,2,3-Tetrachloropropene
| Conditions | Yield |
|---|---|
| With sodium hydroxide; cetylpyridinium bromide at 130℃; for 2h; | 97% |
| With potassium hydroxide | |
| With sodium hydroxide |
- 24425-97-6
1,1,1,2,2,3-hexachloropropane
- 10436-39-2
1,1,2,3-Tetrachloropropene
| Conditions | Yield |
|---|---|
| With hydrogenchloride; zinc In 1,4-dioxane; water at 45℃; for 49h; Autoclave; Inert atmosphere; | 90% |
- 1070-78-6
1,1,1,3-tetrachloropropane
A
- 21700-31-2
1,1,1,2,3-pentachloro-propane
B
- 2567-14-8
3,3-dichloroallyl chloride
C
- 10436-39-2
1,1,2,3-Tetrachloropropene
| Conditions | Yield |
|---|---|
| With iron(III) chloride; chlorine at 82℃; under 1277.21 Torr; for 15.33h; Product distribution / selectivity; | A 82.9% B 3.4% C 8.1% |
- 21700-31-2
1,1,1,2,3-pentachloro-propane
A
- 10436-39-2
1,1,2,3-Tetrachloropropene
B
- 16500-91-7
2,3,3,3-tetrachloropropene
| Conditions | Yield |
|---|---|
| With potassium hydroxide at 0℃; | |
| With potassium hydroxide; Aliquat 336 In water at 80℃; for 3h; | |
| With potassium hydroxide; Aliquat 336 In water at 80℃; for 3h; | |
| With potassium hydroxide; Aliquat 336 In water at 8℃; for 3h; |
- 16500-91-7
2,3,3,3-tetrachloropropene
- 10436-39-2
1,1,2,3-Tetrachloropropene
| Conditions | Yield |
|---|---|
| at 180℃; | |
| With aluminium trichloride at 0℃; | |
| With antimonypentachloride | |
| at 150 - 180℃; |
- 67-56-1
methanol
- 3266-39-5
2,3,3-trichloro-2-propen-1-ol
A
- 80-63-7
methyl 2-chloroacrylate
B
- 10436-39-2
1,1,2,3-Tetrachloropropene
| Conditions | Yield |
|---|---|
| With sulfuric acid; water 1) 105 deg C, 4 h, 2) 30 min; Yield given. Multistep reaction. Yields of byproduct given; |
- 21700-31-2
1,1,1,2,3-pentachloro-propane
A
- 2233-00-3
3,3,3-trichloro-1-propene
B
- 10436-39-2
1,1,2,3-Tetrachloropropene
| Conditions | Yield |
|---|---|
| at 400℃; under 750.075 Torr; for 0.0130556h; Inert atmosphere; |
- 21700-31-2
1,1,1,2,3-pentachloro-propane
A
- 2252-87-1
2,3-dichloro-3,3-difluoroprop-1-ene
B
- 10436-39-2
1,1,2,3-Tetrachloropropene
C
- 666-27-3
1,1,2,3-tetrachloro-1-fluoro-propane
| Conditions | Yield |
|---|---|
| With hydrogen fluoride at 290℃; under 750.075 Torr; for 3h; Inert atmosphere; tubular reactor; |
| Conditions | Yield |
|---|---|
| Stage #1: prop-1-yne With chlorine at 60 - 80℃; Stage #2: With chlorine; dibenzoyl peroxide at 40 - 50℃; Stage #3: With sodium hydroxide at 40 - 50℃; |
| Conditions | Yield |
|---|---|
| at 100 - 450℃; under 1018.63 Torr; Temperature; Reagent/catalyst; Pressure; Inert atmosphere; | 8.1 %Spectr. |
1,1,2,3-Tetrachloropropene Chemical Properties
IUPAC Name: 1,1,2,3-Tetrachloroprop-1-ene
The MF of 1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2) is C3H2Cl4.
The MW of 1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2) is 179.86.
Synonyms of 1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2): Tetrachloropropene ; 1,1,2,3-Tetrachloropropene ; 1,1,2,3-Tetrachloro-1-propene ; 1,1,2,3-Tetrachloro-propen ; 2,3,3-Trichloroallyl chloride
Apperance: Colorless oily liquid
Index of Refraction: 1.512
EINECS: 233-920-8
Density: 1.539 g/ml
Flash Point: 62.3 °C
Boiling Point: 173.8 °C
1,1,2,3-Tetrachloropropene Uses
1,1,2,3-Tetrachloropropene (CAS NO.10436-39-2) is Ye Yan fear herbicide intermediate and used for the synthesis of heat-resistant plastic.
1,1,2,3-Tetrachloropropene Production
A dehydrochlorination: tirring 1,1,2,3 - Tetrachloro-propane,calcium hydroxide and a certain amount of water in the reactors, to a certain reaction temperature for several hours, add 1:1 hydrochloric acid and in to acidic deposition layered collection of mixed-bit three allyl chloride.
Secondary chloride: reaction equipment is the same chlorination, mixed with bits into three allyl chloride, were mixed with bits 5-chloropropane.
Second dehydrochlorination: Production equipment is the same dehydrochlorination in the reaction vessel into position five chlorine mixed with propane, adding calcium hydroxide, dehydrochlorination was four allyl chloride.
ClCH=CHCH2Cl+Cl2→ClCH2CHClCHCl2
ClCH2CHClCHCl2+OH-→ClCH2ClG=CHCl
ClCH2ClC=CHCl+Cl2→Cl2CHCCl2CH2Cl
Cl2CHCCl2CH2Cl+OH-→Cl2C=CClCH2Cl
1,1,2,3-Tetrachloropropene Toxicity Data With Reference
| Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
|---|---|---|---|---|---|
| mouse | LC50 | inhalation | 3200mg/m3 (3200mg/m3) | Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 23(10), Pg. 51, 1979. | |
| mouse | LD50 | oral | 800mg/kg (800mg/kg) | LIVER: OTHER CHANGES | Gigiena i Sanitariya. For English translation, see HYSAAV. Vol. 43(4), Pg. 15, 1978. |
| rabbit | LD50 | oral | 477mg/kg (477mg/kg) | Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 23(10), Pg. 51, 1979. | |
| rabbit | LD50 | skin | 400uL/kg (0.4mL/kg) | American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969. | |
| rat | LC50 | inhalation | 1500mg/m3 (1500mg/m3) | Gigiena Truda i Professional'nye Zabolevaniya. Labor Hygiene and Occupational Diseases. Vol. 23(10), Pg. 51, 1979. | |
| rat | LD50 | oral | 350mg/kg (350mg/kg) | American Industrial Hygiene Association Journal. Vol. 30, Pg. 470, 1969. |
1,1,2,3-Tetrachloropropene Consensus Reports
Reported in EPA TSCA Inventory.
1,1,2,3-Tetrachloropropene Safety Profile
Poison by ingestion and skin contact. Moderately toxic by inhalation. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of Cl−. See also CHLORINATED HYDROCARBONS, ALIPHATIC.
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