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Cas Database |
| Name |
2-(Perfluorohexyl)ethyl methacrylate |
EINECS | 218-407-9 |
| CAS No. | 2144-53-8 | Density | 1.459g/cm3 |
| PSA | 26.30000 | LogP | 5.23460 |
| Solubility | 42μg/L at 20℃ | Melting Point |
N/A |
| Formula | C12H9F13O2 | Boiling Point | 220 °C at 760 mmHg |
| Molecular Weight | 432.181 | Flash Point | 84.6 °C |
| Transport Information | N/A | Appearance | N/A |
| Safety | 26-36 | Risk Codes | 36/37/38 |
| Molecular Structure |
|
Hazard Symbols |
 
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| Synonyms |
Methacrylicacid, 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl ester (7CI,8CI);1-Octanol,3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-, methacrylate (8CI);(Perfluorohexyl)ethyl methacrylate;1H,1H,2H,2H-Perfluorooctyl methacrylate;2-(Perfluorohexyl)ethyl methacrylate;3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctan-1-yl 2-methyl-2-propenoate;3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluorooctyl methacrylate;FAMAC 6;M 1620; |
Article Data | 9 |
2-(Perfluorohexyl)ethyl methacrylate Synthetic route
- 79-41-4
poly(methacrylic acid)
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With hydroquinone; toluene-4-sulfonic acid In toluene at 115℃; for 5h; | 94% |
| With sulfuric acid; hydroquinone In benzene Heating; | |
| With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; |
- 760-93-0
methacryloyl anhydride
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With dmap; triethylamine In dichloromethane; 1,1,2-Trichloro-1,2,2-trifluoroethane at 30℃; for 18h; | 76% |
- 2043-57-4
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
- 5536-61-8
sodium methacrylate
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With tetra-n-butylphosphonium chloride In o-xylene; water at 100℃; for 12h; Reagent/catalyst; | 71.8% |
- 75-25-2
Bromoform
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
- 67-64-1
acetone
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzonitrile; acetonitrile at 20℃; for 5h; | 70% |
- 67-66-3
chloroform
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
- 67-64-1
acetone
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzonitrile; acetonitrile at 50℃; for 42h; | 8.8% |
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
- 920-46-7
Methacryloyl chloride
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With triethylamine In tetrahydrofuran Yield given; |
- 2043-57-4
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
- 6900-35-2
potassium methacrylate
A
- 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol
B
- 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
C
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With 10H-phenothiazine In tert-butyl alcohol at 130 - 170℃; for 6 - 9h; |
- 2043-57-4
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
- 6900-35-2
potassium methacrylate
A
- 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
B
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With 10H-phenothiazine In tert-butyl alcohol at 160℃; for 9h; |
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| at 540℃; for 0.55h; Inert atmosphere; | 1.36 g |
- 31001-77-1
mercaptopropylmethyldimethoxysilane
- 2144-53-8
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
| Conditions | Yield |
|---|---|
| With 2,2'-azobis(isobutyronitrile) In acetonitrile at 80℃; for 4h; | 60% |
2-(Perfluorohexyl)ethyl methacrylate Specification
The 2-(Perfluorohexyl)ethyl methacrylate with its cas register number is 2144-53-8. It also can be called as 1,1,2,2-Tetrahydroperfluorooctyl methacrylate and the IUPAC Name about this chemical is 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylprop-2-enoate. It belongs to the following product categories, such as monomer, Acrylic Monomers, Fluorinated Acrylics, Monomers and so on.
Physical properties about 2-(Perfluorohexyl)ethyl methacrylate are: (1)ACD/LogP: 6.71; (2)# of Rule of 5 Violations: 1; (3)ACD/LogD (pH 5.5): 6.71; (4)ACD/LogD (pH 7.4): 6.71; (5)ACD/BCF (pH 5.5): 74149.32; (6)ACD/BCF (pH 7.4): 74149.32; (7)ACD/KOC (pH 5.5): 106562.2; (8)ACD/KOC (pH 7.4): 106562.2; (9)#H bond acceptors: 2; (10)#Freely Rotating Bonds: 9; (11)Polar Surface Area: 26.3Å2; (12)Index of Refraction: 1.333; (13)Molar Refractivity: 60.9 cm3; (14)Molar Volume: 296.1 cm3; (15)Polarizability: 24.14x10-24cm3; (16)Surface Tension: 18.4 dyne/cm; (17)Enthalpy of Vaporization: 45.64 kJ/mol; (18)Vapour Pressure: 0.116 mmHg at 25°C.
Preparation: this chemical can be prepared by 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctan-1-ol and methacrylic acid-anhydride. This reaction will need reagent DMAP, Et3N and solvent CH2Cl2, 1,1,2-trichloro-1,2,2-trifluoro-ethane . The reaction time is 18 hour(s) with reaction temperature of 30 ℃. The yield is about 76%.
When you are using this chemical, please be cautious about it as the following:
This chemical is irritating to eyes, respiratory system and skin. When you are using it, wear suitable protective clothing. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
You can still convert the following datas into molecular structure:
(1)Canonical SMILES: CC(=C)C(=O)OCCC(C(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F
(2)InChI: InChI=1S/C12H9F13O2/c1-5(2)6(26)27-4-3-7(13,14)8(15,16)9(17,18)10(19,20)11(21,22)12(23,24)25/h1,3-4H2,2H3
(3)InChIKey: CDXFIRXEAJABAZ-UHFFFAOYSA-N
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