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Cas Database |
| Name |
2-Ethyl-2-adamantanol |
EINECS | N/A |
| CAS No. | 14648-57-8 | Density | 1.045 g/cm3 |
| PSA | 20.23000 | LogP | 2.58360 |
| Solubility | N/A | Melting Point |
70 °C |
| Formula | C12H20O | Boiling Point | 265.5 °C at 760 mmHg |
| Molecular Weight | 180.29 | Flash Point | 110.2 °C |
| Transport Information | N/A | Appearance | N/A |
| Safety | 24/25 | Risk Codes | R36/37/38 |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
2-Adamantanol,2-ethyl- (8CI);2-Ethyl-2-hydroxytricyclo[3,3,1,1(3,7)])decane;Tricyclo[3.3.1.13,7]decan-2-ol,2-ethyl-; |
Article Data | 8 |
2-Ethyl-2-adamantanol Synthetic route
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 0℃; for 2h; Inert atmosphere; | 100% |
| Stage #1: 2-Adamantanone; ethyllithium In tetrahydrofuran; diethyl ether; benzene at 0 - 20℃; for 2h; Inert atmosphere; Stage #2: With ammonium chloride In tetrahydrofuran; diethyl ether; water; benzene Inert atmosphere; | 94% |
| In tetrahydrofuran; benzene at 0℃; | 94% |
| In diethyl ether; benzene |
- 700-58-3
2-Adamantanone
- 925-90-6
ethylmagnesium bromide
A
- 700-57-2
1-adamantanol
B
- 14648-57-8
2-ethyl-2-adamantanol
| Conditions | Yield |
|---|---|
| Stage #1: ethylmagnesium bromide With (trimethylsilyl)methylmagnesium chloride; lithium chloride; zinc(II) chloride In tetrahydrofuran; diethyl ether at 20℃; Grignard addition; Stage #2: 2-Adamantanone In tetrahydrofuran; diethyl ether at 0℃; for 3h; Grignard addition; | A 16% B 80% |
| In tetrahydrofuran; diethyl ether at 0℃; Grignard addition; | A 80% B 18% |
- 10467-10-4
ethylmagnesium iodide
- 700-58-3
2-Adamantanone
- 75-03-6
ethyl iodide
A
- 700-57-2
1-adamantanol
B
- 14648-57-8
2-ethyl-2-adamantanol
| Conditions | Yield |
|---|---|
| With magnesium In tetrahydrofuran |
- 14648-57-8
2-ethyl-2-adamantanol
- 14451-87-7
2-ethyladamantane
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid In hexane at 25 - 50℃; for 51h; | 89% |
- 14648-57-8
2-ethyl-2-adamantanol
| Conditions | Yield |
|---|---|
| With sodium azide; trifluoroacetic acid In dichloromethane at 0 - 20℃; for 28h; | 80% |
| With sodium azide; trifluoroacetic acid In dichloromethane at 0 - 20℃; for 28h; | 80% |
| With sodium azide; sulfuric acid; water In chloroform at 0 - 20℃; |
- 14648-57-8
2-ethyl-2-adamantanol
- 74693-81-5
5-(1-iodoethylydene)-4-oxatricyclo<4.3.1.1.3,8>undecane
| Conditions | Yield |
|---|---|
| With lead(IV) acetate; iodine; calcium carbonate In benzene for 3h; Heating; | 33% |
- 14648-57-8
2-ethyl-2-adamantanol
A
- 700-58-3
2-Adamantanone
B
- 66633-37-2
2-Hydroxy-2-adamantyl methyl ketone
| Conditions | Yield |
|---|---|
| With nitric acid; acetic anhydride at 20℃; for 1h; Further byproducts given; | A 32% B 10% C 15% D 19% |
- 14648-57-8
2-ethyl-2-adamantanol
A
- 700-58-3
2-Adamantanone
| Conditions | Yield |
|---|---|
| With nitric acid; acetic anhydride at 20℃; for 1h; Further byproducts given; | A 32% B 7% C 15% D 19% |
- 14648-57-8
2-ethyl-2-adamantanol
- 108-24-7
acetic anhydride
A
- 700-58-3
2-Adamantanone
B
- 66633-37-2
2-Hydroxy-2-adamantyl methyl ketone
| Conditions | Yield |
|---|---|
| With nitric acid at 20℃; for 1h; Further byproducts given; | A 32% B 10% C 15% D 19% |
- 14648-57-8
2-ethyl-2-adamantanol
- 79-04-9
chloroacetyl chloride
- 625122-38-5
2-chloroacetoxy-2-ethyladamantane
| Conditions | Yield |
|---|---|
| With pyridine In tetrahydrofuran at 0 - 20℃; for 24.25h; | 22.2% |
2-Ethyl-2-adamantanol Chemical Properties
Molecular structure of 2-Ethyl-2-adamantanol (CAS NO.14648-57-8) is:
Product Name: 2-Ethyl-2-adamantanol
CAS Registry Number: 14648-57-8
Empirical Formula: C12H20O
Molecular Weight: 180.2866
Melting Point: 70 °C
Surface Tension: 39.7 dyne/cm
Density: 1.045 g/cm3
Flash Point: 110.2 °C
Enthalpy of Vaporization: 58.47 kJ/mol
Boiling Point: 265.5 °C at 760 mmHg
Vapour Pressure: 0.00126 mmHg at 25°C
Product Categories: Adamantane Derivative;Adamantane derivatives;Adamantanes
2-Ethyl-2-adamantanol Specification
2-Ethyl-2-adamantanol , its cas register number is 14648-57-8. It also can be called 2-Ethyl-2-hydroxytricyclo[3,3,1,1(3,7)])decane ; 2-Adamantanol,2-ethyl- (8CI) ; Tricyclo[3.3.1.13,7]decan-2-ol,2-ethyl-.
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