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Boric-10B acid

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Name

Boric-10B acid

EINECS 237-478-7
CAS No. 13813-79-1 Density 1.438 g/cm3
PSA 60.69000 LogP -2.05180
Solubility N/A Melting Point 170.9oC
Formula H310BO3 Boiling Point N/A
Molecular Weight 61.022 Flash Point N/A
Transport Information N/A Appearance N/A
Safety 22-26-36/37/39-45 Risk Codes 36/37/38-62-63
Molecular Structure Molecular Structure of 13813-79-1 (BORIC-10B ACID) Hazard Symbols HarmfulXn
Synonyms

Boric-10Bacid (H310BO3) (6CI,7CI);[10B]Boric acid;

Article Data 2

Boric-10B acid Synthetic route

(10)B2O3

13813-79-1

[10B]boric acid

Conditions
ConditionsYield
(10)B2O3 was dissolved in H2O, evaporation to dryness at room temp.;;
4832-27-3

trimethyl borate-10

13813-79-1

[10B]boric acid

Conditions
ConditionsYield
at 25℃; Activation energy;
13813-79-1

[10B]boric acid

71-36-3

butan-1-ol

207742-80-1

tributyl (10B)borate

Conditions
ConditionsYield
In neat (no solvent) Reflux; Inert atmosphere;96%
Inert atmosphere; Reflux;95%
In toluene byproducts: H2O; (Schlesinger, H. I., et al.; J. Am. Chem. Soc., 1953, v. 75, pp. 216-215); to anhyd. H3(10)BO3 b-BuOH and toluene added; mixt. heated to 130°C over 5 h; distilled at 226-228°C under 1 atm;87%
With sulfuric acid In toluene at 130℃; for 3.5h;73.58%
13813-79-1

[10B]boric acid

7288-07-5

2-methoxy-N,N-bis(2-methoxyphenyl)-aniline

113633-81-1

2,2',2''-nitrilotriphenyl borate

Conditions
ConditionsYield
In toluene byproducts: H2O; heating a mixture of 0.61 g (10-B) boric acid and 3 g 2,2',2''-nitrilotriphenol in 50 ml toluene under reflux, evaporation and sublimation at 300°C, 0.05 Torr;; elem. anal.;;90%
13813-79-1

[10B]boric acid

7789-21-1

fluorosulphonic acid

15875-25-9

boron trifluoride

Conditions
ConditionsYield
room temperature; trap to trap condensation in vacuum, determination of purity by IR;75%
13813-79-1

[10B]boric acid

7782-50-5

chlorine

28098-23-9

boron trichloride

Conditions
ConditionsYield
chlorinated at 560°C;75%
13813-79-1

[10B]boric acid

67-63-0

isopropyl alcohol

[10B]-triisopropoxyborane

Conditions
ConditionsYield
With calcium hydride at 90℃; Inert atmosphere; Schlenk technique;54%
With calcium hydride In neat (no solvent) at 90℃; for 16h; Inert atmosphere;
76-09-5

2,3-dimethyl-2,3-butane diol

13813-79-1

[10B]boric acid

[10B]-pinacolborane

Conditions
ConditionsYield
Stage #1: 2,3-dimethyl-2,3-butane diol; [10B]boric acid In benzene at 100℃; for 10h;
Stage #2: With sodium tetrahydroborate In benzene
35%
78-10-4

tetraethoxy orthosilicate

13813-79-1

[10B]boric acid

86119-84-8, 7664-38-2

phosphoric acid

O2Si(88),(10)BO4P(12) (A%)

O2Si(88),(10)BO4P(12) (A%)

Conditions
ConditionsYield
In neat (no solvent) sol-gel method; accordingly to K. S. Chou, J. Non Cryst. Solids 110 (1989) 122, A. Adamczyk, PhD Thesis, University of Mining and Metallurgy, Krakow, 1999 and A. Adamczyk et al., XXII EUCMOS, Balatonfuered, Hungary, 1996;
78-10-4

tetraethoxy orthosilicate

13813-79-1

[10B]boric acid

86119-84-8, 7664-38-2

phosphoric acid

O2Si(97),(10)BO4P(3) (A%)

O2Si(97),(10)BO4P(3) (A%)

Conditions
ConditionsYield
In neat (no solvent) sol-gel method; accordingly to K. S. Chou, J. Non Cryst. Solids 110 (1989) 122, A. Adamczyk, PhD Thesis, University of Mining and Metallurgy, Krakow, 1999 and A. Adamczyk et al., XXII EUCMOS, Balatonfuered, Hungary, 1996;

Boric-10B acid Specification

The Boric-10B acid, with the CAS registry number 13813-79-1, is also known as (10B)Orthoboric acid. It belongs to the product categories of Alphabetical Listings; B; Stable Isotopes. Its EINECS registry number is 237-478-7. This chemical's molecular formula is H310BO3 and molecular weight is 61.83. Its IUPAC name is called boric acid. This chemical's classification code is TSCA Flag P [A commenced PMN (Premanufacture Notice) substance].

Physical properties of Boric-10B acid: (1)ACD/BCF (pH 5.5): 1; (2)ACD/BCF (pH 7.4): 1; (3)ACD/KOC (pH 7.4): ; (4)#H bond acceptors: 3; (5)#H bond donors: 3; (6)#Freely Rotating Bonds: 3; (7)Index of Refraction: 1.385; (8)Molar Refractivity: 10.083 cm3; (9)Molar Volume: 43.003 cm3; (10)Surface Tension: 59.198 dyne/cm; (11)Density: 1.438 g/cm3.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause damage to health. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing, gloves and eye/face protection. In case of accident or if you feel unwell seek medical advice immediately (show the label where possible).

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: B(O)(O)O
(2)InChI: InChI=1S/BH3O3/c2-1(3)4/h2-4H
(3)InChIKey: KGBXLFKZBHKPEV-UHFFFAOYSA-N

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