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Conditions | Yield |
---|---|
With trichloroacetamide; triphenylphosphine In dichloromethane at 30℃; for 0.25h; | 99% |
Stage #1: 2-phenylethanol With N,N-dimethylthiourea In dichloromethane at 20℃; Stage #2: With N-chloro-succinimide In dichloromethane at 20℃; for 1h; Irradiation; | 98% |
With 1,3,5-trichloro-2,4,6-triazine; N,N-dimethyl-formamide In dichloromethane at 25℃; for 0.25h; | 97% |
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane for 1h; Heating; | A 99% B 97% |
2-phenylethyl mesylate
2-phenylethyl chloride
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium chloride at 50℃; for 1h; Inert atmosphere; Green chemistry; | 98% |
diphenethyl-1,1 trimethylene-4,4' bipiperidine
2-phenylethyl chloride
Conditions | Yield |
---|---|
With phenyl chloroformate In neat (no solvent) Heating; | 93% |
2-phenylethanol
3,3-dichloro-1,2-diphenylcyclopropene
A
2-phenylethyl chloride
B
diphenylcyclopropenone
Conditions | Yield |
---|---|
In dichloromethane at 23℃; for 0.25h; Mechanism; Solvent; Inert atmosphere; | A 89% B n/a |
In dichloromethane at 23℃; for 0.25h; |
2-phenylethanol
Benzotrichlorid
A
benzylidene dichloride
B
2-phenylethyl chloride
Conditions | Yield |
---|---|
With TOP; phenylsilane In neat (no solvent) at 100℃; for 24h; Appel Halogenation; Inert atmosphere; | A n/a B 88% |
1-chloro-4-(2-chloroethyl)benzene
2-phenylethyl chloride
Conditions | Yield |
---|---|
With palladium on activated charcoal; formic acid; N,N-dimethyl-formamide for 5h; Heating; | 85% |
Conditions | Yield |
---|---|
With dichloromethylsilane; iron(III) chloride In 1,2-dimethoxyethane for 4h; Heating; | 85% |
Conditions | Yield |
---|---|
With titanium tetrachloride In 1,2-dichloro-ethane for 3h; Reflux; | 85% |
2-phenylethanol
benzoyl chloride
A
2-Phenylethyl benzoate
B
2-phenylethyl chloride
Conditions | Yield |
---|---|
With 2,3-diethyl-2-cyclopropen-1-one In tert-butyl methyl ether at 40℃; for 15h; | A n/a B 83% |
Product Name: 1-Chloro-2-phenylethane
CAS Registry Number: 622-24-2
IUPAC Name: 1-chloro-2-ethylbenzene
Molecular Weight: 140.61006 [g/mol]
Molecular Formula: C8H9Cl
XLogP3: 3.5
Surface Tension: 33.8 dyne/cm
EINECS: 210-725-6
Density: 1.052 g/cm3
Flash Point: 66.7 °C
Melting Point: -60 °C
Refractive index: n20/D 1.53(lit.)
Water Solubility: 0.1 g/L (20 ºC)
Enthalpy of Vaporization: 41.67 kJ/mol
Boiling Point: 198.2 °C at 760 mmHg
Vapour Pressure: 0.512 mmHg at 25°C
Product Categories: Benzene derivates
Following is the molecular structure of 1-Chloro-2-phenylethane (CAS NO.622-24-2) is:
Safty information about 1-Chloro-2-phenylethane (CAS NO.622-24-2) is:
Hazard Codes:
Xi
Risk Statements:
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements:
S23:Do not breathe vapour.
S24/25:Avoid contact with skin and eyes.
S37/39:Wear suitable gloves and eye/face protection.
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
WGK Germany: 3
HS Code: 29036990
1-Chloro-2-phenylethane (CAS NO.622-24-2) is a clear, colorless liquid.
First Aid Measures about it:
Eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Get medical aid.
Skin: Get medical aid. Flush skin with plenty of water for at least 15 minutes while removing contaminated clothing and shoes.
Ingestion: Get medical aid. Wash mouth out with water.
Inhalation: Remove from exposure and move to fresh air immediately. If not breathing, give artificial respiration. If breathing is difficult, give oxygen. Get medical aid.
Handling and Storage about it:
Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes.
Storage: Keep away from sources of ignition. Store in a cool, dry place. Store in a tightly closed container.