CAS No.10393-86-9,METHANESULFONYL HYDRAZIDE Suppliers

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Basic Information

Molecular Structure:
CAS No.:	10393-86-9
Name:	METHANESULFONYL HYDRAZIDE
Article Data:	16

Formula:	CH₆N₂O₂S
Molecular Weight:	110.137
Synonyms:	Mesyl hydrazide;
EINECS:	-0
Density:	1.401 g/cm³
Melting Point:	46-48 °C
Boiling Point:	229 °C at 760 mmHg
Flash Point:	92.3 °C
Hazard Symbols:	R36/37/38:Irritating to eyes, respiratory system and skin.;
Risk Codes:	36/37/38
Safety:	15-26-36
PSA:	80.57000
LogP:	0.58130

Synthetic route

: 124-63-0
methanesulfonyl chloride

: 10393-86-9
methanesulphonyl hydrazide

Conditions

Conditions	Yield
With sodium hydroxide; hydrazine hydrate In water at 8℃;	90%
With hydrazine hydrate In tetrahydrofuran at 10 - 15℃; for 0.5h;	82%
With hydrazine hydrate In ethanol at 10 - 20℃; for 1h;	50%

: 124-63-0
methanesulfonyl chloride

A: 10393-86-9
methanesulphonyl hydrazide

B: 18300-37-3
di-methanesulfonyl hydrazide

Conditions

Conditions	Yield
With sodium hydroxide; hydrazine hydrate In water cooling;

: 1201-93-0
1-phenyl-3-dimethylaminoprop-2-enone

: 10393-86-9
methanesulphonyl hydrazide

: 3708-04-1
2-methylsulfonyl-1-phenylethanone

Conditions

Conditions	Yield
Stage #1: 1-phenyl-3-dimethylaminoprop-2-enone; methanesulphonyl hydrazide With tert.-butylhydroperoxide In water at 80℃; for 8h; Stage #2: With copper diacetate In water	96%

: 2913-97-5
N-phthalimidyl-2-aminoacetaldehyde

: 10393-86-9
methanesulphonyl hydrazide

: C11H11N3O4S

Conditions

Conditions	Yield
In ethanol at 70℃; for 0.5h; Condensation;	95%

: 292638-84-7
styrene

: 10393-86-9
methanesulphonyl hydrazide

: 15436-11-0
(E)-methyl styryl sulfone

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; iodine; sodium carbonate In toluene at 90℃; for 3h; Inert atmosphere; stereoselective reaction;	95%
With oxygen; copper(l) chloride; lithium bromide In dimethyl sulfoxide at 100℃; under 760.051 Torr; for 12h; Schlenk technique; stereoselective reaction;	88%

: 120-72-9
indole

: 10393-86-9
methanesulphonyl hydrazide

: 2-(methylsulfonyl)-1H-indole

Conditions

Conditions	Yield
With tert.-butylhydroperoxide; iodine In water; 1,2-dichloro-ethane at 20℃; for 2h; Green chemistry;	92%

: 10393-86-9
methanesulphonyl hydrazide

: 51673-84-8
dimethoxyacetaldehyde

A: 917918-89-9
(E)-N'-(2,2-dimethoxyethylidene)methanesulfonohydrazide

B: C4H10N4O4S2

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃; for 3.5h;	A 91.1% B n/a

...Expand

: 119-61-9
benzophenone

: 10393-86-9
methanesulphonyl hydrazide

: 1244620-37-8
N'-(diphenylmethylene)methanesulfonohydrazide

Conditions

Conditions	Yield
With hydrogenchloride In methanol; water for 24h; Reflux;	90%
With hydrogenchloride In methanol; water for 1h; Reflux;

: 10393-86-9
methanesulphonyl hydrazide

: (S)-2-amino-4-phenylbut-3-ene

: C11H14O2S

Conditions

Conditions	Yield
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 20℃; for 24h;	90%

: 10393-86-9
methanesulphonyl hydrazide

: 193536-85-5
(3R,3aS,4R,SR,7S,9R,9aR,12R)-3-methoxy-4,7,9,12-tetramethyl-8-oxo-7-vinyldecahydro-4,9a-propanocyclopenta[8]annulen-5-yl carbonochloridate

: 193536-97-9
(3R)-3-deoxo-11-deoxy-3-methoxy-11-oxo-4-epi-mutilin 14-[N-(methanesulphonylamino) carbamate]

Conditions

Conditions	Yield
In dichloromethane	89%

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Specification

The Methanesulfonic acid,hydrazide, with the CAS registry number of 10393-86-9, is also known as Mesyl hydrazide. Its molecular formula is CH₆N₂O₂S and molecular weight is 110.14. What's more, its IUPAC name is Methanesulfonohydrazide. In addition, it must be stored in airtight containers and placed in a dry, cool place.

Physical properties about the Methanesulfonic acid,hydrazide are: (1)ACD/LogP: -1.47; (2)# of Rule of 5 Violations: 0; (3)#H bond acceptors: 4; (4)#H bond donors: 3; (5)#Freely Rotating Bonds: 1; (6)Polar Surface Area: 49 Å²; (7)Index of Refraction: 1.491; (8)Molar Refractivity: 22.76 cm³; (9)Molar Volume: 78.5 cm³; (10)Surface Tension: 53.1 dyne/cm; (11)Density: 1.401 g/cm³; (12)Flash Point: 92.3 °C; (13)Enthalpy of Vaporization: 46.56 kJ/mol; (14)Boiling Point: 229 °C at 760 mmHg; (15)Vapour Pressure: 0.0711 mmHg at 25 °C.

Preparation: this chemical can be obtained by Methanesulfonyl chloride. The reaction needs reagent Hydrazine hydrate and solvent H₂O. The reaction temperature is 8 °C. The yield is about 90 %.

The Methanesulfonic acid,hydrazide can be obtained by Methanesulfonyl chloride

Uses: it is used to produce other chemicals. For example, it is used to produce Phenyl methaneselenesulfonate. This reaction needs solvent CH₂Cl₂. The reaction time is 30 min. The yield is about 65 %.

The Methanesulfonic acid,hydrazide can react with Benzeneseleninic acid to get Phenyl methaneselenesulfonate

When you are using this chemical, please be cautious about it as the following:
As a chemical, it is irritating to eyes, respiratory system and skin. If contact with eyes accidently, rinse immediately with plenty of water and seek medical advice. In addition, during using it, wear suitable protective clothing.

You can still convert the following datas into molecular structure:
(1) SMILES: O=S(=O)(NN)C
(2) InChI: InChI=1/CH6N2O2S/c1-6(4,5)3-2/h3H,2H2,1H3
(3) InChIKey: VKHZYWVEBNIRLX-UHFFFAOYAS