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| CAS No.: | 121-97-1 |
|---|---|
| Name: | Methoxypropiophenone |
| Article Data: | 223 |
| Molecular Structure: | |
|
|
|
| Formula: | C10H12O2 |
| Molecular Weight: | 164.204 |
| Synonyms: | p-Methoxypropiophenone;4-Methoxypropiophenone;Propiophenone,4'-methoxy- (6CI,7CI,8CI);Propiophenone, p-methoxy- (4CI);1-(4-Methoxyphenyl)-1-propanone;1-Methoxy-4-propanoylbenzene;4-Propanoylanisole;4'-Methoxypropiophenone;Ethyl 4-methoxyphenyl ketone;Ethyl p-methoxyphenyl ketone;NSC 11834; |
| EINECS: | 204-512-7 |
| Density: | 1.071 g/cm3 |
| Melting Point: | 27-29 °C(lit.) |
| Boiling Point: | 272.316 °C at 760 mmHg |
| Flash Point: | 118.806 °C |
| Appearance: | Clear colourless to amber liquid |
| Hazard Symbols: |
 Xi
|
| Safety: | 24/25 |
| Transport Information: | UN 1993 |
| PSA: | 26.30000 |
| LogP: | 2.28790 |
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| Conditions | Yield |
|---|---|
| With Noccaea caerulescens extract supported in montmorillonite K10 at 60℃; for 6h; Friedel Crafts acylation; Inert atmosphere; regioselective reaction; | 100% |
| With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 2.5h; | 98% |
| With benzyltributylammonium tetrachloroferrate at 50℃; for 0.1h; Friedel-Crafts reaction; | 93% |
| Conditions | Yield |
|---|---|
| With lithium perchlorate at 60℃; for 1h; | 99% |
| Stage #1: methoxybenzene; propionic acid anhydride With modified ZSM-5 zeolite at 100℃; for 5h; Stage #2: at 500℃; for 2h; Temperature; Calcination; | 97.6% |
| With hafnium(IV) trifluoromethanesulfonate; lithium perchlorate In nitromethane for 6h; Ambient temperature; | 93% |
- 51410-44-7
1-(4-methoxylphenyl)-2-propen-1-ol
- 121-97-1
4-Methoxypropiophenone
| Conditions | Yield |
|---|---|
| With tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate; potassium carbonate In acetonitrile for 1h; Inert atmosphere; Reflux; | 99% |
| With [Ru(η(3):η(3)-C10H16)Cl(O2CCH3)] In aq. phosphate buffer at 50℃; for 1h; pH=7; Sealed tube; Inert atmosphere; | 99% |
| With Fe(II)(bis(2-(diisopropylphosphino)ethyl)amine)(CO)(H)(Cl); potassium tert-butylate In toluene at 80℃; for 1h; Inert atmosphere; | 98% |
| Conditions | Yield |
|---|---|
| With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(ll) dichloride; potassium carbonate In tetrahydrofuran; tert-butyl methyl ether at 20℃; for 24h; Inert atmosphere; Schlenk technique; | 99% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In 1,2-dimethoxyethane at 145℃; for 0.416667h; Microwave irradiation; Inert atmosphere; Sealed vessel; | 98% |
| With potassium carbonate at 150 - 160℃; for 4h; | 81% |
- 92409-14-8
C17H20O4
- 121-97-1
4-Methoxypropiophenone
| Conditions | Yield |
|---|---|
| With 5%-palladium/activated carbon; ammonium formate In ethanol; water at 80℃; for 1h; | 98% |
- 5349-60-0
1-(4-methoxyphenyl)-1-propanol
A
- 623-12-1
4-chloromethoxybenzene
B
- 121-97-1
4-Methoxypropiophenone
| Conditions | Yield |
|---|---|
| With dichloromethane extract derived from 6percent aqueous hypochlorite/tetra-n-butylammonium bisulfate solution with pH value to 8-9 In dichloromethane at 20℃; | A 92% B 6% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetonitrile for 20.5h; Heating / reflux; | 89% |
| With sodium hydroxide | |
| With hydroxide |
- 94607-41-7
(E)-1-(4-methoxyphenyl)-3-chloropropene
- 121-97-1
4-Methoxypropiophenone
| Conditions | Yield |
|---|---|
| With potassium carbonate; phenylboronic acid; [Ru(cyclopentadienyl)(MeCN)3]PF6 In acetonitrile at 20℃; for 16h; | 89% |
| With cyclopentadienylruthenium(II) trisacetonitrile hexafluorophosphate; potassium carbonate; phenylboronic acid In acetonitrile at 20℃; for 24h; Inert atmosphere; regioselective reaction; | 89% |
- 52898-49-4
4,N-dimethoxy-N-methylbenzamide
- 925-90-6
ethylmagnesium bromide
- 121-97-1
4-Methoxypropiophenone
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at 0 - 5℃; for 1h; Weinreb Ketone Synthesis; Inert atmosphere; | 89% |
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Chemistry
IUPAC Name: 1-(4-Methoxyphenyl)propan-1-one
Systematic of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): 4'-Methoxypropiophenone ; AI3-04094 ; EINECS 204-512-7 ; Ethyl 4-methoxyphenyl ketone ; NSC 11834 ; p-Methoxypropiophenone ; Propiophenone, 4'-methoxy- (8CI)
CAS NO: 121-97-1
Molecular Formula of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): C10H12O2
Molecular Weight: 164.2011
Molecular Structure:
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Melting Point: 27-29 °C
H bond acceptors: 2
Freely Rotating Bonds: 3
Polar Surface Area: 26.3 Å2
Index of Refraction: 1.501
Molar Refractivity: 47.59 cm3
Molar Volume: 161.4 cm3
Surface Tension: 33.6 dyne/cm
Density of 1-Propanone,1-(4-methoxyphenyl)- (CAS NO.121-97-1): 1.016 g/cm3
Flash Point: 118.8 °C
Enthalpy of Vaporization: 51.06 kJ/mol
Boiling Point: 272.3 °C at 760 mmHg
Vapour Pressure: 0.00612 mmHg at 25°C
Safety Profile
Hazard Codes: 
Xi
Safety Statements: 24/25
S24/25: Avoid contact with skin and eyes.
RIDADR: 1993
WGK Germany: 3
Hazard Note: Irritant