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131276-24-9

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Basic Information
CAS No.: 131276-24-9
Name: 1,8-Bis(diphenylphosphino)anthra
Article Data: 4
Molecular Structure:
Molecular Structure of 131276-24-9 (1,8-Bis(diphenylphosphino)anthra)
Formula: C14H8Br2
Molecular Weight: 336.026
Synonyms: 1,8-Bis(diphenylphosphino)anthra;1,8-Bis(diphenylphosphino)anthracene
Density: 1.768±0.06 g/cm3(Predicted)
Melting Point: 166.0 to 170.0 °C
Boiling Point: 438.8±18.0 °C(Predicted)
PSA: 0.00000
LogP: 0.00000
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Conditions
ConditionsYield
With Al(c-C6H11O)3; cyclohexanol for 72h; Heating;77%
Stage #1: 1,8-dibromoanthraquinone With sodium tetrahydroborate In methanol at -78℃;
Stage #2: With hydrogenchloride In methanol Heating;
Stage #3: With sodium tetrahydroborate In methanol; diethylene glycol dimethyl ether at 20℃;		6.6 g
With aluminum isopropoxide; cyclohexanol for 72h; Reflux;
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1,8-dibromo-10-anthrone

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1,8-dibromoanthraquinone

Conditions
ConditionsYield
Stage #1: 1,8-dibromo-10-anthrone With sodium tetrahydroborate In propan-1-ol
Stage #2: With hydrogenchloride		76%
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1,8-dichloroanthraquinone

131276-24-9

1,8-dibromoanthraquinone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 62 percent / CuCl2; KBr; H3PO4 / nitrobenzene / Heating
2.1: sodium borohydride / methanol / -78 °C
2.2: HCl / methanol / Heating
2.3: 6.6 g / sodium borohydride / bis-(2-methoxy-ethyl) ether; methanol / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: CuCl2; KBr; H3PO4 / nitrobenzene / Heating
2.1: sodium borohydride / methanol / -78 °C
2.2: HCl / methanol / Heating
2.3: 6.6 g / sodium borohydride / bis-(2-methoxy-ethyl) ether; methanol / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: potassium bromide; copper dichloride; phosphoric acid / nitrobenzene / 48 h / Reflux
2: aluminum isopropoxide; cyclohexanol / 72 h / Reflux
View Scheme
131276-24-9

1,8-dibromoanthraquinone

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p-benzoquinone

C20H12Br2O2

Conditions
ConditionsYield
In isopropyl alcohol Schlenk technique; Inert atmosphere; Reflux;96%
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4-(propionyl)phenylboronic acid pinacol ester

131276-24-9

1,8-dibromoanthraquinone

C32H26O2

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate; catacxium A In 1,2-dimethoxyethane; water at 85℃; for 20h; Suzuki-Miyaura Coupling; Inert atmosphere;95%
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Benzophenone imine

131276-24-9

1,8-dibromoanthraquinone

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N1,N8-bis(diphenylmethylene)anthracene-1,8-diamine

Conditions
ConditionsYield
With 1,8-bis(diisopropylphosphino)triptycene; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0) In toluene Buchwald-Hartwig amination;93%
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1,8-dibromoanthraquinone

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N,N-dimethyl-formamide

1202642-07-6

8-bromo-anthracene-1-carbaldehyde

Conditions
ConditionsYield
Stage #1: 1,8-dibromoanthraquinone With phenyllithium In tetrahydrofuran; dibutyl ether at -78℃; for 1.16667h; Inert atmosphere;
Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; dibutyl ether at -78 - 20℃; for 1h; Inert atmosphere;		92%

3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

131276-24-9

1,8-dibromoanthraquinone

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Conditions
ConditionsYield
With di(1-adamantyl)-n-butylphosphine; palladium diacetate; potassium carbonate In 1,2-dimethoxyethane; water at 85℃; for 20h; Inert atmosphere;88%
131276-24-9

1,8-dibromoanthraquinone

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N-boc-2-pyrroleboronic acid

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Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 18h; Suzuki Coupling; Reflux;84%
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4-(carbazol-9-yl)phenylboronic acid

131276-24-9

1,8-dibromoanthraquinone

1,8-bis[4-(9R-carbazole-9-yl)phenyl]anthracene

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 14h; Inert atmosphere;83%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 90℃; for 14h;
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    Shandong Jiashisheng Biotechnolgy Co.,Ltd is located in high-tech Zone, Liaocheng City, Shandong Province, China, old factory was found in 2008, also named Jiashisheng Group. Here

  • Shandong Jiashisheng Biotechnolgy Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:13165407087

    Address:Bock B, Yunshang Building, High-tech Zone

       Inquiry Now

  • OLED Intermediates 1,8-Bis(diphenylphosphino)anthra

  • Casno:

    131276-24-9

    OLED Intermediates 1,8-Bis(diphenylphosphino)anthra

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Our company has been engaged in the Pharmaceutical raw material and pharmaceutical intermediates medicine material intermediates and related chemical industry for more than ten ye

  • Taizhou volsen chemical Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-576-88869393

    Address:Jiaojiang District, Taizhou, Zhejiang, China.

       Inquiry Now

  • Anthracene, 1,8-dibromo-

  • Casno:

    131276-24-9

    Anthracene, 1,8-dibromo-

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    good quality, cheap price and stable quantityAppearance:white powder Storage:at room temperature Package:1g;5g;10g;100g; Application:OLED intermediates Transportation:BY AIR

    Wuhan HengHeDa Pharm Co., Ltd is a hi-tech enterprise locates in Wuhan Private Science and Technology Park, specializing in custom synthesis, manufacture and import & export of fin

  • Wuhan HengHeDa Pharm Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-27-84888681

    Address:Wuhan economic & technology development zone

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  • 131276-24-9

  • Casno:

    131276-24-9

    131276-24-9

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    OLED Intermediates 1,8-Bis(diphenylphosphino)anthra Application:OLED Material

    We are Hebei minshang biotechnology co. LTD., mainly deal in pharmaceutical intermediates and various chemicals. We are manufacturers and have our own factory. Products & Usage Ph

  • Hebei Minshang Biotechnology Co., Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18032092709

    Address:hebei

       Inquiry Now

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