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14721-66-5

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Basic Information
CAS No.: 14721-66-5
Name: PHYTANIC ACID
Article Data: 17
Molecular Structure:
Molecular Structure of 14721-66-5 (PHYTANIC ACID)
Formula: C20H40 O2
Molecular Weight: 312.536
Synonyms: Phytanicacid (6CI); 3,7,11,15-Tetramethylhexadecanoic acid; NSC 108698; Phytanoic acid
Density: 0.88 g/cm3
Melting Point: -65°C
Boiling Point: 422.3 °C at 760 mmHg
Flash Point: 179.7 °C
Appearance: Clear colorless liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
PSA: 37.30000
LogP: 6.53630
Related products
Synthetic route
645-72-7

3,7,11,15-tetramethyl-hexadecanol

14721-66-5

phytanic acid

Conditions
ConditionsYield
With potassium permanganate; tetrabutylammomium bromide; acetic acid In water; 1,2-dichloro-ethane at 16℃; for 4.5h; Reflux;94%
With potassium permanganate; tetrabutylammomium bromide; acetic acid In water; 1,2-dichloro-ethane at 16℃; for 4.5h; Reflux;94%
With potassium permanganate; tetrabutylammomium bromide; acetic acid In water; 1,2-dichloro-ethane at 16℃; for 4.5h; Reflux;94%
60-29-7

diethyl ether

645-72-7

3,7,11,15-tetramethyl-hexadecanol

14721-66-5

phytanic acid

Conditions
ConditionsYield
With sodium disulfite; chromic acid; acetic acid In [(2)H6]acetone; water72.3%
220904-31-4

3,7,11,15-tetramethyl-2-hexadecen-1-oic acid

14721-66-5

phytanic acid

Conditions
ConditionsYield
With platinum Hydrogenation;
102464-52-8

2,6,10,14-Tetramethyl-pentadecanon-(12)-carbonsaeure-(1)

14721-66-5

phytanic acid

Conditions
ConditionsYield
With potassium hydroxide; hydrazine hydrate; diethylene glycol at 195℃;
645-72-7

3,7,11,15-tetramethyl-hexadecanol

A

14721-66-5

phytanic acid

B

phytanic acid dihydrophytyl ester

phytanic acid dihydrophytyl ester

7541-49-3

3,7,11,15-tetramethyl-2-hexadecen-1-ol

14721-66-5

phytanic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Katalitrische Hydrierung.Hydrogenation
2: chromic acid; glacial acetic acid; KHSO4
View Scheme
Multi-step reaction with 2 steps
1: platinum(IV) oxide; hydrogen / tetrahydrofuran / 4 h / 20 °C / 750.08 Torr
2: tetrabutylammomium bromide; acetic acid; potassium permanganate / water; 1,2-dichloro-ethane / 4.5 h / 16 °C / Reflux
View Scheme
Multi-step reaction with 2 steps
1: hydrogen; platinum(IV) oxide / tetrahydrofuran / 4 h / 20 °C / 750.08 Torr
2: tetrabutylammomium bromide; acetic acid; potassium permanganate / water; 1,2-dichloro-ethane / 4.5 h / 16 °C / Reflux
View Scheme
Multi-step reaction with 2 steps
1: hydrogen; platinum(IV) oxide / tetrahydrofuran / 4 h / 20 °C / 750.08 Torr
2: tetrabutylammomium bromide; acetic acid; potassium permanganate / water; 1,2-dichloro-ethane / 4.5 h / 16 °C / Reflux
View Scheme
102899-50-3

2,6,10,14-Tetramethyl-pentadecanon-(12)-carbonsaeure-(1)-methylester

14721-66-5

phytanic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / methanol
2: KOH, diethylene glycol, aq. N2H4 / 195 °C
View Scheme
150-86-7

phytol

14721-66-5

phytanic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen / water; ethanol / 72 h / 20 °C
2: Jones reagent / acetone / 0.5 h / 0 °C
View Scheme
14721-66-5

phytanic acid

2133-40-6

L-proline methyl ester monohydrochloride

C26H49NO3

Conditions
ConditionsYield
Stage #1: phytanic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In chloroform at 20℃; for 0.25h;
Stage #2: L-proline methyl ester monohydrochloride In chloroform at 20℃; for 18h;		95%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In chloroform at 0 - 20℃; for 18.25h;95%
Stage #1: phytanic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In chloroform at 20℃; for 0.25h;
Stage #2: L-proline methyl ester monohydrochloride In chloroform at 20℃; for 18h;		95%
14721-66-5

phytanic acid

2133-40-6

L-proline methyl ester monohydrochloride

C26H49NO3

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 18.25h;95%
Raw Materials
645-72-7
7541-49-3
60-29-7
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32607-05-9
1189-37-3
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