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16526-56-0

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Basic Information
CAS No.: 16526-56-0
Name: 2-methyladenosine
Article Data: 15
Molecular Structure:
Molecular Structure of 16526-56-0 (2-methyladenosine)
Formula: C11H15 N5 O4
Molecular Weight: 281.271
Synonyms: 2-Methyladenosine;NSC 93499
Density: 1.96g/cm3
Boiling Point: 517.8°Cat760mmHg
Flash Point: 266.9°C
PSA: 139.54000
LogP: -1.09040
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Synthetic route
23192-64-5

5-amino-1-β-D-ribofuranosyl-1H-imidazole-4-carbonitrile

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
In ammonia methyl alcohol; acetonitrile35.9%
108-24-7

acetic anhydride

1445-08-5

2-methyl-6-aminopurine

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
Behandeln des Reaktionsprodukts mit wss.NaOH und HgCl2 in Aethanol, Erhitzen der entstandenen Chloromercurio-Verb. mit Tri-O-acetyl-α-D-ribofuranosylchlorid in Xylol und anschlissenden Behandeln mit methanol.NH3;
75-24-1

trimethylaluminum

146-76-9

2-Bromo-adenosine

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
Yield given. Multistep reaction;

Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-(6-amino-2-methyl-purin-9-yl)-tetrahydro-furan-3-yl ester

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
With ammonia In methanol
With potassium carbonate In methanol at 23℃; for 12h;
107-71-1

tert-butyl peroxyacetate

58-61-7

adenosine

A

56973-12-7

8-methyladenosine

B

16526-56-0

2-methyladenosine

C

1867-73-8

N6-methyladenosine

Conditions
ConditionsYield
at 32℃; for 20h; Product distribution; Mechanism; Irradiation; solutions of pH 1.4-12.4;
...Expand

N-(4,6-diamino-2-methyl-pyrimidin-5-yl)-formamide

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: formamide
2: Behandeln des Reaktionsprodukts mit wss.NaOH und HgCl2 in Aethanol, Erhitzen der entstandenen Chloromercurio-Verb. mit Tri-O-acetyl-α-D-ribofuranosylchlorid in Xylol und anschlissenden Behandeln mit methanol.NH3
View Scheme
5473-05-2

2-methyl-5-phenylazo-pyrimidine-4,6-diyldiamine

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: palladium/charcoal; water / Hydrogenation
2: formamide
3: Behandeln des Reaktionsprodukts mit wss.NaOH und HgCl2 in Aethanol, Erhitzen der entstandenen Chloromercurio-Verb. mit Tri-O-acetyl-α-D-ribofuranosylchlorid in Xylol und anschlissenden Behandeln mit methanol.NH3
View Scheme
75-24-1

trimethylaluminum

35109-88-7

2-iodoadenosine

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
Stage #1: 2-iodoadenosine With ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane at 80℃;
Stage #2: trimethylaluminum; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran; hexanes at 68℃; for 3.66h;
Stage #3: With water; ammonium chloride In methanol at 65℃; for 3h;
53293-86-0

C20H39N5O4Si3

16526-56-0

2-methyladenosine

Conditions
ConditionsYield
With water; ammonium chloride In methanol
16526-56-0

2-methyladenosine

A

18646-11-2

α-D-ribofuranosyl-1-phosphate

B

1445-08-5

2-methyladenine

Conditions
ConditionsYield
With E. coli purine nucleoside phosphorylase Enzyme kinetics; Substitution;
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