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CAS No.: | 31140-40-6 |
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Name: | 4-METHOXYCARBONYLPHENYL CHLOROFORMATE |
Article Data: | 7 |
Molecular Structure: | |
Formula: | C9H7 Cl O4 |
Molecular Weight: | 214.605 |
Synonyms: | Benzoicacid, p-hydroxy-, methyl ester, chloroformate (8CI); 4-Methoxycarbonylphenylchloroformate; 4-[(Chlorocarbonyl)oxy]benzoic acid methyl ester;p-Carbomethoxyphenyl chloroformate; p-Methoxycarbonylphenyl chloroformate |
Density: | 1.342g/cm3 |
Melting Point: | 51-54oC |
Boiling Point: | 283.3°Cat760mmHg |
Flash Point: | 120°C |
PSA: | 52.60000 |
LogP: | 2.21080 |
Conditions | Yield |
---|---|
With quinoline; benzene | |
In benzene | |
With pyridine In toluene | |
With quinoline; toluene |
methyl 4-[(chlorocarbonyl)oxy]benzoate
1,2-(2,3-dihydro-1H-azirino)-<60>fullerene
Conditions | Yield |
---|---|
With pyridine In various solvent(s) at 70℃; for 1h; | 78% |
1-cyanopyrazolidine
methyl 4-[(chlorocarbonyl)oxy]benzoate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 45.2% |
methyl 4-[(chlorocarbonyl)oxy]benzoate
Conditions | Yield |
---|---|
With pyridine In acetonitrile at 0 - 20℃; Inert atmosphere; | 32% |
Conditions | Yield |
---|---|
With pyridine In acetonitrile B12(OH)12(2-), chloroformate, pyridine, acetonitrile (excess), 96 h, room temp.; filtered, the solvent was removed under vac., the residue was pptd. fromCH2Cl2 with diethyl ether, benchtop flash column chromy. using gradient of CH2Cl2 and CH3CN over neutral alumina; | 32% |
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran at 20℃; Inert atmosphere; | 30% |
methyl 4-[(chlorocarbonyl)oxy]benzoate
1,4-diazabicyclo[3.2.2]nonane
Conditions | Yield |
---|---|
25% |
1-cyanohexahydropyridazine
methyl 4-[(chlorocarbonyl)oxy]benzoate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 1% |
methyl 4-[(chlorocarbonyl)oxy]benzoate
2-(Diethylamino)ethanol
Conditions | Yield |
---|---|
With benzene | |
With benzene |
methyl 4-[(chlorocarbonyl)oxy]benzoate
2-(Diethylamino)ethanol
B
dimethyl 4,4′-(carbonylbis(oxy))dibenzoate
Conditions | Yield |
---|---|
With benzene |