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| CAS No.: | 6305-04-0 |
|---|---|
| Name: | 2-CHLORO-4'-HYDROXYACETOPHENONE |
| Article Data: | 24 |
| Molecular Structure: | |
|
|
|
| Formula: | C8H7 Cl O2 |
| Molecular Weight: | 170.595 |
| Synonyms: | Acetophenone,2-chloro-4'-hydroxy- (6CI,7CI); 2-Chloro-1-(4-hydroxyphenyl)ethanone;2-Chloro-4'-hydroxyacetophenone; 4-Hydroxy-a-chloroacetophenone; 4-Hydroxyphenacyl chloride;4'-Hydroxy-2-chloroacetophenone; Chlorophenacyle; NSC 41671;p-(Chloroacetyl)phenol; p-Hydroxyphenacyl chloride; w-Chloro-4-hydroxyacetophenone |
| EINECS: | 228-613-0 |
| Density: | 1.304 g/cm3 |
| Melting Point: | 145-146 °C |
| Boiling Point: | 337.1 ºC at 760 mmHg |
| Flash Point: | 157.7 ºC |
| Safety: | A poison by ingestion. A severe skin and eye irritant. When heated to decomposition it emits toxic vapors of Cl−. |
| PSA: | 37.30000 |
| LogP: | 1.81370 |
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| Conditions | Yield |
|---|---|
| With N,N,N-trimethylbenzenemethanaminium dichloroiodate In methanol; 1,2-dichloro-ethane for 10h; Heating; | 95% |
| With 2,2,3,4,5,6-hexachloro-cyclohexa-2,4-dien-1-one In ethanol for 5h; Heating; | 77% |
| With hydrogenchloride; ammonium nitrate; iodine; oxygen In water; acetonitrile at 60℃; for 22h; Green chemistry; chemoselective reaction; | 64% |
| With N-chloro-succinimide; toluene-4-sulfonic acid In acetonitrile at 40℃; | 45% |
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride In dichloromethane at 0 - 30℃; for 7h; Solvent; | 94% |
| With aluminium trichloride In various solvent(s) at 70℃; for 5h; | 50% |
| Stage #1: chloroacetyl chloride; phenol; aluminum (III) chloride In 1,2-dichloro-ethane at 0 - 65℃; for 13h; Stage #2: With hydrogenchloride In dichloromethane; water | 15% |
- 868746-76-3
2-chloro-1-(4-chloroacetoxy-phenyl)-ethanone
- 6305-04-0
p-hydroxyphenacyl chloride
| Conditions | Yield |
|---|---|
| With sodium hydroxide In methanol; water at 0 - 20℃; for 0.5h; | 85% |
| Conditions | Yield |
|---|---|
| With beryllium(II) chloride at 130 - 140℃; | |
| With aluminium trichloride at 120℃; |
| Conditions | Yield |
|---|---|
| With aluminium trichloride |
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methoxybenzene
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chloroacetyl chloride
A
- 53074-73-0
2-(2-chloroacetyl)phenol
B
- 6305-04-0
p-hydroxyphenacyl chloride
| Conditions | Yield |
|---|---|
| With aluminium trichloride; 1,1,2,2-tetrachloroethane | |
| With aluminium trichloride; 1,1,2,2-tetrachloroethane |
| Conditions | Yield |
|---|---|
| With aluminium trichloride; Petroleum ether | |
| With aluminium trichloride | |
| With carbon disulfide; aluminium trichloride | |
| With aluminium trichloride |
- 6305-04-0
p-hydroxyphenacyl chloride
| Conditions | Yield |
|---|---|
| at 110℃; |
| Conditions | Yield |
|---|---|
| at 120℃; |
| Conditions | Yield |
|---|---|
| With aluminium trichloride at 120℃; |
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Chemistry
IUPAC Name: 2-Chlor-1-(4-hydroxyphenyl)ethanon
The MF of 2-Chlor-1-(4-hydroxyphenyl)ethanon (6305-04-0) is C8H7ClO2.
The MW of 2-Chlor-1-(4-hydroxyphenyl)ethanon (6305-04-0) is 170.59298.
Synonyms of 2-Chlor-1-(4-hydroxyphenyl)ethanon (6305-04-0): 2-Chloro-1-(4-hydroxyphenyl)ethanone ; Ethanone, 2-chloro-1- (4-hydroxyphenyl)- ; 2-Chloro-1-(4-hydroxyphenyl)ethan-1-one ; 2-Chloro-4'-hydroxyacetophenone
Index of Refraction: 1.571
EINECS: 228-613-0
Density: 1.304 g/ml
Flash Point: 157.7 °C
Boiling Point: 337.1 °C
Toxicity Data With Reference
| 1. | skn-rbt 500 mg SEV | JACTDZ Journal of the American College of Toxicology. 12 (1993),581. | ||
| 2. | eye-rbt 10 mg SEV | JACTDZ Journal of the American College of Toxicology. 12 (1993),581. | ||
| 3. | orl-rat LD50:230 mg/kg | JACTDZ Journal of the American College of Toxicology. 12 (1993),581. | ||
| 4. | skn-rbt LD50:>8 g/kg | JACTDZ Journal of the American College of Toxicology. 12 (1993),581. |
Safety Profile
A poison by ingestion. A severe skin and eye irritant. When heated to decomposition it emits toxic vapors of Cl−.