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CAS No.: | 766-33-6 |
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Name: | 1,3-Dioxane, 2,5,5-trimethyl- |
Article Data: | 7 |
Molecular Structure: | |
Formula: | C7H14O2 |
Molecular Weight: | 130.187 |
Synonyms: | 1,3-Dioxane,2,5,5-trimethyl;2,2,5-trimethyl-1,3-dioxane; |
Density: | 0.886g/cm3 |
Boiling Point: | 132.883°C at 760 mmHg |
Flash Point: | 33.968°C |
PSA: | 18.46000 |
LogP: | 1.40540 |
Conditions | Yield |
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In dichloromethane at 20℃; for 3h; | A 79% B n/a |
Conditions | Yield |
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In dichloromethane at 20℃; for 3h; | A 59% B n/a |
Conditions | Yield |
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In dichloromethane at 20℃; for 3h; | A 54% B n/a |
Conditions | Yield |
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With zinc(II) chloride | A 5% B n/a |
Conditions | Yield |
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In dichloromethane for 1h; Product distribution; Ambient temperature; | A 22 % Chromat. B n/a |
diethyl acetal
2-isobutyl-5,5-dimethyl-1,3,2-dioxaborinane
2,5,5-trimethyl-1,3-dioxane
Conditions | Yield |
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With zinc(II) chloride transacetalation; |
Conditions | Yield |
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sulfuric acid at 20℃; for 1h; Condensation; |
diisobutyl ester of isobutylboronic acid
2,5,5-trimethyl-1,3-dioxane
Conditions | Yield |
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Multi-step reaction with 2 steps 1: ZnCl2 / 0.08 h / 130 °C 2: ZnCl2 View Scheme | |
Multi-step reaction with 2 steps 1: ZnCl2 / 0.08 h / 130 °C 2: ZnCl2 View Scheme | |
Multi-step reaction with 2 steps 1: ZnCl2 / 2 h / 130 °C 2: ZnCl2 View Scheme |
Conditions | Yield |
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In diethyl ether for 0.25h; Heating; | 82% |
2,5,5-trimethyl-1,3-dioxane
allyl-trimethyl-silane
[2,2-Dimethyl-3-(1-methyl-but-3-enyloxy)-propoxy]-trimethyl-silane
Conditions | Yield |
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With zinc(II) iodide at 100℃; for 4h; | 75% |