USD $5.00-10.00 / Gram
USD $1.00-10.00 / Kilogram
USD $1.00-10.00 / Kilogram
USD $2.00-10.00 / Kilogram
USD $2.00-10.00 / Kilogram
USD $2.00-10.00 / Kilogram
USD $1.00-10.00 / Kilogram
USD $1.00-10.00 / Kilogram
USD $1.00-10.00 / Kilogram
test items |
acceptance criteria |
result |
conclusion |
characters |
a white or almost white crystalline powder |
white crystalline powder |
conform |
identification |
the ir spectrum conforms to that obtained with the reference substance. |
the ir spectrum conforms to that obtained with the reference substance. |
conform |
its solution gives reaction(a) of chlorides |
its solution gives reaction(a) of chlorides |
conform |
|
appearance of solution |
clear and not more intensely coloured than reference solution y6 |
clear and not more intensely coloured than reference solution y6 |
conform |
ph |
3.5~5.5 |
4.9 |
conform |
specific optical rotation |
+135º~+150º |
+141º |
conform |
related substances |
impurity a ≤0.5% |
0.3% |
conform |
impurity b ≤0.5% |
0.2% |
||
impurity c ≤0.2% |
0.03% |
||
any unspecified impurity≤0.10% |
0.02% |
||
total impurities:≤2.0% |
0.2% |
||
heavy metals |
not more than 5ppm |
less than 5ppm |
conform |
water |
3.1%~4.6% |
3.9% |
conform |
sulfated ash |
not more than 0.5% |
0.2% |
conform |
bacterial endotoxins |
less than 0.50 iu/mg |
less than 0.50 iu/mg |
conform |
residual solvents |
n-butanol: not more than 5000ppm |
undetected |
conform |
acetone not more than 0.5% |
0.05% |
||
assay ( on anhydrous basis) |
lincomycin b maximum 5.0% |
2.7% |
|
sum of the contents of lincomycin hydrochloride and lincomycin b hydrochloride: 96.0%-102.0%; |
100.1% |
conform |