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Name	10-Methoxyiminostilbene	EINECS	225-172-6
CAS No.	4698-11-7	Density	1.19 g/cm³
PSA	21.26000	LogP	4.02610
Solubility	N/A	Melting Point	122-128 °C
Formula	C₁₅H₁₃NO	Boiling Point	410.8 °C at 760 mmHg
Molecular Weight	223.274	Flash Point	162.5 °C
Transport Information	N/A	Appearance	Yellowish foam
Safety		Risk Codes	N/A
Molecular Structure		Hazard Symbols	N/A
Synonyms	10-Oxo-10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxamide;10-Methoxy-5H-dibenz(b,f)azepine;	Article Data	19

10-Methoxyiminostilbene Synthetic route

: 353497-37-7
10-methoxy-5H-dibenz[b,f]azepine-5-carboxylic acid methyl ester

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
With sodium hydroxide In various solvent(s) at 100℃; for 4h;	98%
With sodium hydroxide In water	98%
With sodium hydroxide In methanol; water at 105 - 110℃; for 2.5h;	97%

: 731851-94-8
10-methoxy-dibenzo[b,f]azepine-5-carboxylic acid phenyl ester

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
With sodium hydroxide In various solvent(s) at 100℃; for 4h;	96%

: 10465-66-4
5-benzyl-10-methoxyiminostilbene

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
With 5%-palladium/activated carbon; hydrogen at 35 - 40℃; under 1500.15 - 2250.23 Torr; for 5h; Autoclave;	93.5%

: 153261-62-2
5-acetyl-10-methoxy-5H-dibenzazepine

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
With potassium hydroxide In ethylene glycol for 5h; Heating;	80%
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube;	67%
Stage #1: 5-acetyl-10-methoxy-5H-dibenzazepine With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 6h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction;	59%

: 5-allyl-10-methoxy-5H-dibenzo[b,f]azepine

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
With potassium tert-butylate In dimethyl sulfoxide

: 5-formyl-10-bromo-11-methoxy-10,11-dihydro-5H-dibenzo[b,f]azepine

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
Stage #1: 5-formyl-10-bromo-11-methoxy-10,11-dihydro-5H-dibenzo[b,f]azepine With 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene for 0.5h; Heating / reflux; Stage #2: With Deloxan ASP I/7; potassium hydroxide In toluene Product distribution / selectivity; Heating / reflux;

: 39507-06-7
(2-phenylamino-phenyl)-acetic acid methyl ester

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: pyridine / toluene / 24 h / 50 °C 1.2: pyridine / 22 h / 100 °C 2.1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 3.1: 70 percent / polyphosphoric acid / 3 h / 95 °C 4.1: 81 percent / p-TsOH / methanol / 5 h / Heating 5.1: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C View Scheme
Multi-step reaction with 6 steps 1: pyridine / toluene / 24 h / 50 °C 2: pyridine / 22 h / 100 °C 3: sodium hydroxide / water; methanol / 24 h / 20 °C 4: polyphosphoric acid / 3 h / 90 - 95 °C 5: water / 0 - 98 °C 6: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C View Scheme

: 353497-31-1
10,11-dihydro-10-oxo-5H-dibenz[b,f]azepine-5-carboxylic acid methyl ester

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 81 percent / p-TsOH / methanol / 5 h / Heating 2: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C View Scheme
Multi-step reaction with 2 steps 1: water / 0 - 98 °C 2: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C View Scheme

: 805236-74-2
[2-(methoxycarbonyl-phenyl-amino)-phenyl]-acetic acid methyl ester

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C 2: 70 percent / polyphosphoric acid / 3 h / 95 °C 3: 81 percent / p-TsOH / methanol / 5 h / Heating 4: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C View Scheme
Multi-step reaction with 4 steps 1: sodium hydroxide / water; methanol / 24 h / 20 °C 2: polyphosphoric acid / 3 h / 90 - 95 °C 3: water / 0 - 98 °C 4: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C View Scheme

: 353497-35-5
2-[(methoxycarbonyl)phenylamino]benzeneacetic acid

: 4698-11-7
10-methoxy-5H-dibenzo[b,f]azepine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 70 percent / polyphosphoric acid / 3 h / 95 °C 2: 81 percent / p-TsOH / methanol / 5 h / Heating 3: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C View Scheme
Multi-step reaction with 3 steps 1: polyphosphoric acid / 3 h / 90 - 95 °C 2: water / 0 - 98 °C 3: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C View Scheme

10-Methoxyiminostilbene Chemical Properties

Molecular Structure of 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7):

Molecular Formula: C₁₅H₁₃NO
Molecular Weight: 223.2698
IUPAC Name: 6-Methoxy-11H-benzo[b][1]benzazepine
Synonyms of 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7): EINECS 225-172-6 ; 10-Methoxyiminostilbene ; 10-Methoxy-2,2'-iminostilbene
CAS NO: 4698-11-7
Product Categories: Stilbenes (substituted) ; Aromatics Compounds ; Aromatics ; Heterocycles
Melting point: 122-128°C
Index of Refraction: 1.651
Molar Refractivity: 68.37 cm³
Molar Volume: 187 cm³
Surface Tension: 49.8 dyne/cm
Density: 1.19 g/cm³
Flash Point: 162.5 °C
Enthalpy of Vaporization: 66.32 kJ/mol
Boiling Point: 410.8 °C at 760 mmHg
Vapour Pressure of 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7): 5.86E-07 mmHg at 25°C

10-Methoxyiminostilbene Uses

10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7) is used as Drug Oxcarbazepine.

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